1-(3-{[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-hydroxymethyl-methyl-silanyl}-propyl)-5-methyl-1H-pyrimidine-2,4-dione

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Chemical Name:1-(3-{[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-hydroxymethyl-methyl-silanyl}-propyl)-5-methyl-1H-pyrimidine-2,4-dione
CAS No.:191086-93-8
Molecular Formula:C₃₂H₃₈N₂O₆Si
Molecular Weight:574.749
Hs Code.:

Synonyms:1-(3-{[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-hydroxymethyl-methyl-silanyl}-propyl)-5-methyl-1H-pyrimidine-2,4-dione

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Chemical Property of 1-(3-{[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-hydroxymethyl-methyl-silanyl}-propyl)-5-methyl-1H-pyrimidine-2,4-dione

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Technology Process of 1-(3-{[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-hydroxymethyl-methyl-silanyl}-propyl)-5-methyl-1H-pyrimidine-2,4-dione

There total 7 articles about 1-(3-{[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-hydroxymethyl-methyl-silanyl}-propyl)-5-methyl-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 158610-56-1
1-[3-(Bis-hydroxymethyl-methyl-silanyl)-propyl]-5-methyl-1H-pyrimidine-2,4-dione

: 191086-93-8
1-(3-{[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-hydroxymethyl-methyl-silanyl}-propyl)-5-methyl-1H-pyrimidine-2,4-dione

Guidance literature:: In pyridine; for 4h; Ambient temperature;
DOI:10.1021/jo962165p

Reference yield:

: 65-71-4,28806-14-6,691841-57-3
thymin

: 191086-93-8
1-(3-{[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-hydroxymethyl-methyl-silanyl}-propyl)-5-methyl-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 7 steps

1: ammonium sulfate / Heating

2: 64 percent / dimethylformamide / 72 h / 80 °C

3: trimethylchlorosilane, ammonium sulfate / 5 h / Heating

4: 35 percent / H₂PtCl₆, propan-2-ol / tetrahydrofuran / Heating

5: 72 percent / dimethylformamide / 24 h / 100 - 140 °C

6: 76 percent / K₂CO₃ / methanol / Ambient temperature

7: 48 percent / pyridine / 4 h / Ambient temperature

With dihydrogen hexachloroplatinate; ammonium sulfate; chloro-trimethyl-silane; potassium carbonate; isopropyl alcohol; In tetrahydrofuran; pyridine; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo962165p

Reference yield:

: 158610-61-8
1-[3-(Bis-chloromethyl-methyl-silanyl)-propyl]-5-methyl-1H-pyrimidine-2,4-dione

: 191086-93-8
1-(3-{[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-hydroxymethyl-methyl-silanyl}-propyl)-5-methyl-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / dimethylformamide / 24 h / 100 - 140 °C

2: 76 percent / K₂CO₃ / methanol / Ambient temperature

3: 48 percent / pyridine / 4 h / Ambient temperature

With potassium carbonate; In pyridine; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo962165p