C₄₄H₅₆O₂Si₂

Base Information

Chemical Name:C₄₄H₅₆O₂Si₂
CAS No.:915315-62-7
Molecular Formula:C₄₄H₅₆O₂Si₂
Molecular Weight:673.098
Hs Code.:

C<sub>44</sub>H<sub>56</sub>O<sub>2</sub>Si<sub>2</sub>

Synonyms:C₄₄H₅₆O₂Si₂

Suppliers and Price of C₄₄H₅₆O₂Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₄H₅₆O₂Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₄H₅₆O₂Si₂

There total 11 articles about C₄₄H₅₆O₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 915315-68-3
(3S,4R)-3,4-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-3,4-dimethyl-cyclohexanone

: 915315-62-7
C₄₄H₅₆O₂Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: para-toluenesulfonic acid monohydrate / tetrahydrofuran / 1 h / Heating

2.1: lithium hydride / tetrahydrofuran; toluene / 65 h

2.2: N-bromosuccinimide; dibenzoylperoxide / CCl₄ / 0.75 h

2.3: 15.0 g / potassium tert-butoxide; tetrabutyltinhydride; 2,2'-azobisisobutyronitrile / tetrahydrofuran / 77 h / Heating

With lithium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1021/ol061962z

Reference yield:

: 915315-58-1
(4'aR,8'aS)-dimethyl-1',3',4',5',8',8'a-hexahydro-spiro[[1,3]dioxolane-2,2'-naphthalene]

: 915315-62-7
C₄₄H₅₆O₂Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: ozone gas / CH₂Cl₂; methanol / 0.58 h / -78 °C

1.2: 15.0 g / sodium borohydride / CH₂Cl₂; methanol / 30 h / -15 °C

2.1: 31.0 g / 4-dimethylaminopyridine / dimethylformamide; various solvent(s) / 24 h / 20 °C

3.1: para-toluenesulfonic acid monohydrate / acetone; H₂O / 3 h / Heating

4.1: para-toluenesulfonic acid monohydrate / tetrahydrofuran / 1 h / Heating

5.1: lithium hydride / tetrahydrofuran; toluene / 65 h

5.2: N-bromosuccinimide; dibenzoylperoxide / CCl₄ / 0.75 h

5.3: 15.0 g / potassium tert-butoxide; tetrabutyltinhydride; 2,2'-azobisisobutyronitrile / tetrahydrofuran / 77 h / Heating

With dmap; lithium hydride; toluene-4-sulfonic acid; ozone; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1021/ol061962z

Reference yield:

: 915315-57-0
(8'aS)-methyl-1',3',4',5',8',8'a-hexahydro-spiro[[1,3]dioxolane-2,2'-naphthalene]-(4'aS)-carbonitrile

: 915315-62-7
C₄₄H₅₆O₂Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: diisobutylaluminum hydride / toluene / 2 h

2.1: hydrazine hydrate; hydrazine dihydrochloride / triethylene glycol / 1 h / 130 °C

3.1: 8.55 g / KOH / 220 °C

4.1: ozone gas / CH₂Cl₂; methanol / 0.58 h / -78 °C

4.2: 15.0 g / sodium borohydride / CH₂Cl₂; methanol / 30 h / -15 °C

5.1: 31.0 g / 4-dimethylaminopyridine / dimethylformamide; various solvent(s) / 24 h / 20 °C

6.1: para-toluenesulfonic acid monohydrate / acetone; H₂O / 3 h / Heating

7.1: para-toluenesulfonic acid monohydrate / tetrahydrofuran / 1 h / Heating

8.1: lithium hydride / tetrahydrofuran; toluene / 65 h

8.2: N-bromosuccinimide; dibenzoylperoxide / CCl₄ / 0.75 h

8.3: 15.0 g / potassium tert-butoxide; tetrabutyltinhydride; 2,2'-azobisisobutyronitrile / tetrahydrofuran / 77 h / Heating

With dmap; potassium hydroxide; hydrazine dihydrochloride; lithium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; ozone; hydrazine hydrate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol;
DOI:10.1021/ol061962z