(2R,6R)-N²,N⁶-bis(fluoren-9-ylmethoxycarbonyl)lanthionine α-allyl ester

Base Information

Chemical Name:(2R,6R)-N²,N⁶-bis(fluoren-9-ylmethoxycarbonyl)lanthionine α-allyl ester
CAS No.:881996-32-3
Molecular Formula:C₃₉H₃₆N₂O₈S
Molecular Weight:692.789
Hs Code.:

(2R,6R)-N<sup>2</sup>,N<sup>6</sup>-bis(fluoren-9-ylmethoxycarbonyl)lanthionine α-allyl ester

Synonyms:(2R,6R)-N²,N⁶-bis(fluoren-9-ylmethoxycarbonyl)lanthionine α-allyl ester

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Chemical Property of (2R,6R)-N²,N⁶-bis(fluoren-9-ylmethoxycarbonyl)lanthionine α-allyl ester

Chemical Property:

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Technology Process of (2R,6R)-N²,N⁶-bis(fluoren-9-ylmethoxycarbonyl)lanthionine α-allyl ester

There total 7 articles about (2R,6R)-N²,N⁶-bis(fluoren-9-ylmethoxycarbonyl)lanthionine α-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73724-45-5
N-(9H-fluoren-9-ylmethoxycarbonyl)-L-serine

: 881996-32-3
(2R,6R)-N²,N⁶-bis(fluoren-9-ylmethoxycarbonyl)lanthionine α-allyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisopropylcarbodiimide; CuCl / 120 h

1.2: 65 percent / CH₂Cl₂; dimethylformamide / 4 h / 20 °C

2.1: 84.8 percent / CBr₄; PPh₃ / CH₂Cl₂ / 2 h / 20 °C

3.1: DIEA / dimethylformamide / 4 h / 20 °C

4.1: 2.78 g / TFA / 1 h / 20 °C

With carbon tetrabromide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; copper(l) chloride; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050585d

Reference yield:

: 103213-32-7,167015-11-4
N-(9-fluorenylmethoxycarbonyl)-S-trityl-L-cysteine

: 881996-32-3
(2R,6R)-N²,N⁶-bis(fluoren-9-ylmethoxycarbonyl)lanthionine α-allyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / DIEA / acetonitrile / 16 h / 20 °C

2: 95.1 percent / TFA; triisopropylsilane / CH₂Cl₂; diethyl ether / 1 h / 20 °C

3: DIEA / dimethylformamide / 4 h / 20 °C

4: 2.78 g / TFA / 1 h / 20 °C

With chlorotriisopropylsilane; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm050585d

Reference yield:

: 640722-84-5
allyl 2(R)-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(tritylthio)propanoate

: 881996-32-3
(2R,6R)-N²,N⁶-bis(fluoren-9-ylmethoxycarbonyl)lanthionine α-allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95.1 percent / TFA; triisopropylsilane / CH₂Cl₂; diethyl ether / 1 h / 20 °C

2: DIEA / dimethylformamide / 4 h / 20 °C

3: 2.78 g / TFA / 1 h / 20 °C

With chlorotriisopropylsilane; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050585d