<<3,3,5,5-tetramethyl-4-(1-methylethenyl)-cyclohexenyl>methyl>triphenylphosphonium methanesulfonate

Base Information

Chemical Name:<<3,3,5,5-tetramethyl-4-(1-methylethenyl)-cyclohexenyl>methyl>triphenylphosphonium methanesulfonate
CAS No.:113831-22-4
Molecular Formula:CH₃O₃S*C₃₂H₃₈P
Molecular Weight:548.726
Hs Code.:

Synonyms:<<3,3,5,5-tetramethyl-4-(1-methylethenyl)-cyclohexenyl>methyl>triphenylphosphonium methanesulfonate

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Chemical Property of <<3,3,5,5-tetramethyl-4-(1-methylethenyl)-cyclohexenyl>methyl>triphenylphosphonium methanesulfonate

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Technology Process of <<3,3,5,5-tetramethyl-4-(1-methylethenyl)-cyclohexenyl>methyl>triphenylphosphonium methanesulfonate

There total 2 articles about <<3,3,5,5-tetramethyl-4-(1-methylethenyl)-cyclohexenyl>methyl>triphenylphosphonium methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 603-35-0
triphenylphosphine

: 113831-20-2
3,3,5,5-tetramethyl-1-methylene-4-(1-methylethenyl)-2-methylsulfonylcyclohexane

: 113831-22-4
<<3,3,5,5-tetramethyl-4-(1-methylethenyl)-cyclohexenyl>methyl>triphenylphosphonium methanesulfonate

Guidance literature:: In chloroform; at 50 ℃; for 20h;

Reference yield:

: 81517-76-2
2,2,4,4-tetramethyl-6-methylene-3-(1-methylethenyl)-trans-cyclohexan-1-ol

: 113831-22-4
<<3,3,5,5-tetramethyl-4-(1-methylethenyl)-cyclohexenyl>methyl>triphenylphosphonium methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DMAP / pyridine / 24 h / 0 °C

2: 87 percent / CHCl₃ / 20 h / 50 °C

With dmap; In pyridine; chloroform;