1-(2-methoxy-phenyl)-5,7-dimethyl-3,4-dihydro-naphthalene-2-carboxylic acid

Base Information

Chemical Name:1-(2-methoxy-phenyl)-5,7-dimethyl-3,4-dihydro-naphthalene-2-carboxylic acid
CAS No.:443305-24-6
Molecular Formula:C₂₀H₂₀O₃
Molecular Weight:308.377
Hs Code.:

Synonyms:1-(2-methoxy-phenyl)-5,7-dimethyl-3,4-dihydro-naphthalene-2-carboxylic acid

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Chemical Property of 1-(2-methoxy-phenyl)-5,7-dimethyl-3,4-dihydro-naphthalene-2-carboxylic acid

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Technology Process of 1-(2-methoxy-phenyl)-5,7-dimethyl-3,4-dihydro-naphthalene-2-carboxylic acid

There total 4 articles about 1-(2-methoxy-phenyl)-5,7-dimethyl-3,4-dihydro-naphthalene-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 443305-27-9
1-(2-methoxy-phenyl)-5,7-dimethyl-3,4-dihydro-naphthalene-2-carbaldehyde

: 443305-24-6
1-(2-methoxy-phenyl)-5,7-dimethyl-3,4-dihydro-naphthalene-2-carboxylic acid

Guidance literature:: With sodium chlorite; dihydrogen peroxide; In acetonitrile; at 20 ℃;
DOI:10.1016/S0040-4039(01)02373-5

Reference yield:

: 13621-25-5
5,7-dimethyltetralone

: 443305-24-6
1-(2-methoxy-phenyl)-5,7-dimethyl-3,4-dihydro-naphthalene-2-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / POCl₃

2: 89 percent / K₂CO₃; Bu₄NBr; Pd(OAc)2 / H₂O / 45 °C

3: 96 percent / NaClO₂; H₂O₂ / acetonitrile / 20 °C

With palladium diacetate; sodium chlorite; tetrabutylammomium bromide; dihydrogen peroxide; potassium carbonate; trichlorophosphate; In water; acetonitrile; 1: Vilsmeier-Haack Reaction / 2: Suzuki Coupling;
DOI:10.1016/S0040-4039(01)02373-5

Reference yield:

: 5720-06-9
2-Methoxyphenylboronic acid

: 443305-24-6
1-(2-methoxy-phenyl)-5,7-dimethyl-3,4-dihydro-naphthalene-2-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / K₂CO₃; Bu₄NBr; Pd(OAc)2 / H₂O / 45 °C

2: 96 percent / NaClO₂; H₂O₂ / acetonitrile / 20 °C

With palladium diacetate; sodium chlorite; tetrabutylammomium bromide; dihydrogen peroxide; potassium carbonate; In water; acetonitrile; 1: Suzuki Coupling;
DOI:10.1016/S0040-4039(01)02373-5