N-<2-<<2-ethyl>(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Pentamethyl Ester

Base Information

Chemical Name:N-<2-<<2-ethyl>(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Pentamethyl Ester
CAS No.:126216-34-0
Molecular Formula:C₂₆H₄₀N₄O₁₀
Molecular Weight:568.624
Hs Code.:

N-<2-<<2-<Bis(carboxymethyl)amino>ethyl>(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Pentamethyl Ester

Synonyms:N-<2-<<2-ethyl>(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Pentamethyl Ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-<<2-ethyl>(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Pentamethyl Ester

Chemical Property:

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Technology Process of N-<2-<<2-ethyl>(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Pentamethyl Ester

There total 4 articles about N-<2-<<2-ethyl>(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Pentamethyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 126255-26-3
N-<2-<<2-ethyl>(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-4-nitro-DL-phenylalanine Pentamethyl Ester

: 126216-34-0
N-<2-<<2-ethyl>(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Pentamethyl Ester

Guidance literature:: With tin(ll) chloride; In methanol; for 5h; Heating;
DOI:10.1080/00397919508015498

Reference yield:

: 67-43-6,84932-15-0
diethylenetriaminopentaacetic acid

: 126216-34-0
N-<2-<<2-ethyl>(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Pentamethyl Ester

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / SOCl₂ / 16 h

2: 1) LDA / 1) THF, -78 deg C, 20 min, 2) HMPA, 12 h, -78 deg C -> 25 deg C

3: 1) 97percent H₂SO₄, conc. HNO₃, 2) SOCl₂ / 1) 0 deg C, 3 h, 2) 0 deg C, 14 h

4: H₂ / 30percent Pd/C / methanol / 3 h / 3102.9 Torr

With thionyl chloride; sulfuric acid; hydrogen; nitric acid; lithium diisopropyl amide; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00296a057

Reference yield:

: 126216-31-7
N-<2-<<2-ethyl>(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-DL-phenylalanine Pentamethyl Ester

: 126216-34-0
N-<2-<<2-ethyl>(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Pentamethyl Ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 97percent H₂SO₄, conc. HNO₃, 2) SOCl₂ / 1) 0 deg C, 3 h, 2) 0 deg C, 14 h

2: H₂ / 30percent Pd/C / methanol / 3 h / 3102.9 Torr

With thionyl chloride; sulfuric acid; hydrogen; nitric acid; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00296a057