C₇₁H₁₁₈O₁₀Si₄

Base Information

Chemical Name:C₇₁H₁₁₈O₁₀Si₄
CAS No.:1268269-08-4
Molecular Formula:C₇₁H₁₁₈O₁₀Si₄
Molecular Weight:1244.05
Hs Code.:

C<sub>71</sub>H<sub>118</sub>O<sub>10</sub>Si<sub>4</sub>

Synonyms:C₇₁H₁₁₈O₁₀Si₄

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Chemical Property of C₇₁H₁₁₈O₁₀Si₄

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Technology Process of C₇₁H₁₁₈O₁₀Si₄

There total 15 articles about C₇₁H₁₁₈O₁₀Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1268269-07-3
C₂₇H₄₆O₄Si

: 1268269-06-2
C₄₄H₇₄O₇Si₃

: 1268269-08-4
C₇₁H₁₁₈O₁₀Si₄

Guidance literature:: With dmap; 2-methyl-6-nitrobenzoic anhydride; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja200089f

Reference yield:

: C₃₃H₄₆O₅Si

: 1268269-08-4
C₇₁H₁₁₈O₁₀Si₄

Guidance literature:: Multi-step reaction with 6 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere

2: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

3: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran; tert-butyl alcohol / 6 h / 20 °C / Inert atmosphere

4: lead(IV) tetraacetate / benzene / 0.5 h / 20 °C / Inert atmosphere

5: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene; water / tetrahydrofuran; tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

6: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 20 °C / Inert atmosphere

With dmap; sodium chlorite; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; 2-methyl-6-nitrobenzoic anhydride; water; lead(IV) tetraacetate; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; dichloromethane; toluene; tert-butyl alcohol; benzene;
DOI:10.1021/ja200089f

Reference yield:

: 1268269-16-4
C₃₃H₄₈O₅Si

: 1268269-08-4
C₇₁H₁₁₈O₁₀Si₄

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

2: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran; tert-butyl alcohol / 6 h / 20 °C / Inert atmosphere

3: lead(IV) tetraacetate / benzene / 0.5 h / 20 °C / Inert atmosphere

4: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene; water / tetrahydrofuran; tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

5: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 20 °C / Inert atmosphere

With dmap; sodium chlorite; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; 2-methyl-6-nitrobenzoic anhydride; water; lead(IV) tetraacetate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; dichloromethane; tert-butyl alcohol; benzene;
DOI:10.1021/ja200089f