3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonitril

Base Information

Chemical Name:3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonitril
CAS No.:116527-81-2
Molecular Formula:C₃₃H₃₅N₃O₃
Molecular Weight:521.659
Hs Code.:

Synonyms:3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonitril

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Chemical Property of 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonitril

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Technology Process of 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonitril

There total 7 articles about 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 143-33-9,25596-52-5
sodium cyanide

: 116527-82-3,116562-96-0
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-7-acetoxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol

: 116527-81-2
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonitril

Guidance literature:: With tetrabutylammomium bromide; sodium iodide; In toluene; for 4h; Heating;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-78-7,116556-53-7
2-(3-benzyloxypropyl)-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol-3-on

: 116527-81-2
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonitril

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Lithium aluminium hydride / tetrahydrofuran / 1 h / Heating

2: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

With lithium aluminium tetrahydride; water; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-74-3,116527-77-6
2-(3-benzyloxypropyl)-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol-2-carbonsaure

: 116527-81-2
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonitril

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / 200 - 210 °C

2: 98 percent / Lithium aluminium hydride / tetrahydrofuran / 1 h / Heating

3: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

With lithium aluminium tetrahydride; water; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)86862-9