7-{2-[3,5-bis(methoxymethoxy)phenyl]vinyl}-5-methoxy-1,1,4a-trimethyl-2,3,4,4a,9,9a-hexahydro-1H-xanthen-2-ol

Base Information

Chemical Name:7-{2-[3,5-bis(methoxymethoxy)phenyl]vinyl}-5-methoxy-1,1,4a-trimethyl-2,3,4,4a,9,9a-hexahydro-1H-xanthen-2-ol
CAS No.:865761-94-0
Molecular Formula:C₂₉H₃₈O₇
Molecular Weight:498.617
Hs Code.:

Synonyms:7-{2-[3,5-bis(methoxymethoxy)phenyl]vinyl}-5-methoxy-1,1,4a-trimethyl-2,3,4,4a,9,9a-hexahydro-1H-xanthen-2-ol

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Chemical Property of 7-{2-[3,5-bis(methoxymethoxy)phenyl]vinyl}-5-methoxy-1,1,4a-trimethyl-2,3,4,4a,9,9a-hexahydro-1H-xanthen-2-ol

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Technology Process of 7-{2-[3,5-bis(methoxymethoxy)phenyl]vinyl}-5-methoxy-1,1,4a-trimethyl-2,3,4,4a,9,9a-hexahydro-1H-xanthen-2-ol

There total 4 articles about 7-{2-[3,5-bis(methoxymethoxy)phenyl]vinyl}-5-methoxy-1,1,4a-trimethyl-2,3,4,4a,9,9a-hexahydro-1H-xanthen-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 817592-71-5
{[3,5-bis(methoxymethoxy)phenyl]methyl}phosphonic acid diethyl ester

: 844868-78-6
(7R,8aR,10aR)-7-Hydroxy-4-methoxy-8,8,10a-trimethyl-5,7,8,8a,9,10a-hexahydro-6H-xanthene-2-carbaldehyde

: 865761-94-0
7-{2-[3,5-bis(methoxymethoxy)phenyl]vinyl}-5-methoxy-1,1,4a-trimethyl-2,3,4,4a,9,9a-hexahydro-1H-xanthen-2-ol

Guidance literature:: With 15-crown-5; sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 10h;
DOI:10.1016/j.bmc.2005.10.025

Reference yield:

: 865762-03-4
1-(iodomethyl)-3,5-bis(methoxymethoxy)benzene

: 865761-94-0
7-{2-[3,5-bis(methoxymethoxy)phenyl]vinyl}-5-methoxy-1,1,4a-trimethyl-2,3,4,4a,9,9a-hexahydro-1H-xanthen-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 734 mg / 20 h / 100 °C

2: 91 percent / NaH; 15-crown-5 / tetrahydrofuran / 10 h / 0 - 20 °C

With 15-crown-5; sodium hydride; In tetrahydrofuran; 1: Arbuzov reaction;
DOI:10.1016/j.bmc.2005.10.025

Reference yield:

: methanesulfonic acid 3,5-bis-methoxymethoxy-benzyl ester

: 865761-94-0
7-{2-[3,5-bis(methoxymethoxy)phenyl]vinyl}-5-methoxy-1,1,4a-trimethyl-2,3,4,4a,9,9a-hexahydro-1H-xanthen-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: NaI / acetone / 24 h / 20 °C

2: 734 mg / 20 h / 100 °C

3: 91 percent / NaH; 15-crown-5 / tetrahydrofuran / 10 h / 0 - 20 °C

With 15-crown-5; sodium hydride; sodium iodide; In tetrahydrofuran; acetone; 2: Arbuzov reaction;
DOI:10.1016/j.bmc.2005.10.025