β-allyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-benzylpiperazinylamide

Base Information

Chemical Name:β-allyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-benzylpiperazinylamide
CAS No.:368443-78-1
Molecular Formula:C₃₃H₃₅N₃O₅
Molecular Weight:553.658
Hs Code.:

Synonyms:β-allyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-benzylpiperazinylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-allyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-benzylpiperazinylamide

Chemical Property:

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Technology Process of β-allyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-benzylpiperazinylamide

There total 2 articles about β-allyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-benzylpiperazinylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2759-28-6
1-phenylmethylpiperazine

: 3-(9H-fluoren-9-ylmethoxycarbonylamino)-4-isobutoxycarbonyloxy-4-oxo-butyric acid allyl ester

: 368443-78-1
β-allyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-benzylpiperazinylamide

Guidance literature:: With 4-methyl-morpholine; In tetrahydrofuran; at 0 - 20 ℃; for 4h;
DOI:10.1039/b100401h

Reference yield:

: 177609-12-0
N-alpha-(9-fluorenylmethyloxycarbonyl)-D-aspartic acid beta-allyl ester

: 368443-78-1
β-allyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-benzylpiperazinylamide

Guidance literature:: Multi-step reaction with 2 steps

1: NMM / tetrahydrofuran / 0.08 h / -15 °C

2: 763 mg / NMM / tetrahydrofuran / 4 h / 0 - 20 °C

With 4-methyl-morpholine; In tetrahydrofuran;
DOI:10.1039/b100401h