Boc-Ala-γPhe(β-CH2NO2)-COOEt

Base Information

Chemical Name:Boc-Ala-γPhe(β-CH2NO2)-COOEt
CAS No.:1417890-94-8
Molecular Formula:C₂₂H₃₃N₃O₇
Molecular Weight:451.52
Hs Code.:

Synonyms:Boc-Ala-γPhe(β-CH2NO2)-COOEt

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Chemical Property of Boc-Ala-γPhe(β-CH2NO2)-COOEt

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Technology Process of Boc-Ala-γPhe(β-CH2NO2)-COOEt

There total 4 articles about Boc-Ala-γPhe(β-CH2NO2)-COOEt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 15761-38-3
L-N-Boc-Ala

: C₁₄H₂₀N₂O₄

: 1417890-94-8
Boc-Ala-γPhe(β-CH2NO2)-COOEt

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In ethyl acetate; N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1039/c2ob27070f

Reference yield:

: 124818-94-6,116246-06-1
ethyl (2E,4S)-4-[(tert-butoxycarbonyl)amino]-5-phenylpent-2-enoate

: 1417890-94-8
Boc-Ala-γPhe(β-CH2NO2)-COOEt

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / neat liquid / 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 1 h / 0 °C

3: dicyclohexyl-carbodiimide; benzotriazol-1-ol / ethyl acetate; N,N-dimethyl-formamide / 12 h / 20 °C

With benzotriazol-1-ol; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 1: |Michael Addition;
DOI:10.1039/c2ob27070f

Reference yield:

: 155224-48-9
(3R,4S)-ethyl-4-(tert-butoxycarbonylamino)-3-(nitromethyl)-5-phenyl pentanoate

: 1417890-94-8
Boc-Ala-γPhe(β-CH2NO2)-COOEt

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 0 °C

2: dicyclohexyl-carbodiimide; benzotriazol-1-ol / ethyl acetate; N,N-dimethyl-formamide / 12 h / 20 °C

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c2ob27070f