Technology Process of C39H56N2O7
There total 3 articles about C39H56N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C12H10O4;
With
triethylamine; isobutyl chloroformate;
In
chloroform;
at 20 ℃;
Inert atmosphere;
Cooling with ice;
C27H48N2O4;
In
chloroform;
at 20 ℃;
for 48h;
Inert atmosphere;
DOI:10.1021/jo102577a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 4 h / 20 °C
2.1: triethylamine; isobutyl chloroformate / chloroform / 20 °C / Inert atmosphere; Cooling with ice
2.2: 48 h / 20 °C / Inert atmosphere
With
lithium hydroxide monohydrate; triethylamine; isobutyl chloroformate;
In
tetrahydrofuran; methanol; chloroform; water;
DOI:10.1021/jo102577a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 80 °C / Inert atmosphere
2.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 4 h / 20 °C
3.1: triethylamine; isobutyl chloroformate / chloroform / 20 °C / Inert atmosphere; Cooling with ice
3.2: 48 h / 20 °C / Inert atmosphere
With
lithium hydroxide monohydrate; potassium carbonate; triethylamine; potassium iodide; isobutyl chloroformate;
In
tetrahydrofuran; methanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/jo102577a
