7a-morpholin-4-yl-3-phenyl-4,4a,5,6,7,7a-hexahydro-cyclopenta[e][1,2]oxazine

Base Information

• Chemical Name: 7a-morpholin-4-yl-3-phenyl-4,4a,5,6,7,7a-hexahydro-cyclopenta[e][1,2]oxazine
• CAS No.: 29441-71-2
• Molecular Formula: C₁₇H₂₂N₂O₂
• Molecular Weight: 286.374

Synonyms:7a-morpholin-4-yl-3-phenyl-4,4a,5,6,7,7a-hexahydro-cyclopenta[e][1,2]oxazine

Chemical Property of 7a-morpholin-4-yl-3-phenyl-4,4a,5,6,7,7a-hexahydro-cyclopenta[e][1,2]oxazine

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Technology Process of 7a-morpholin-4-yl-3-phenyl-4,4a,5,6,7,7a-hexahydro-cyclopenta[e][1,2]oxazine

There total 1 articles about 7a-morpholin-4-yl-3-phenyl-4,4a,5,6,7,7a-hexahydro-cyclopenta[e][1,2]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1-(N-morpholino)cyclopent-1-ene (936-52-7) + 2-bromo-1-phenyl-ethanone oxime (14181-72-7,17082-13-2,17082-14-3) → 7a-morpholin-4-yl-3-phenyl-4,4a,5,6,7,7a-hexahydro-cyclopenta[e][1,2]oxazine (29441-71-2)

Guidance literature:

In toluene; for 3h; Ambient temperature;

DOI:10.1246/bcsj.63.3595 DOI:10.1246/cl.1981.869

Reference yield: 53.0%

7a-morpholin-4-yl-3-phenyl-4,4a,5,6,7,7a-hexahydro-cyclopenta[e][1,2]oxazine (29441-71-2) → 4,5-dihydro-2-phenylcyclopentapyrrole (79379-48-9)

Guidance literature:

With triiron dodecarbonyl; trifluoroacetic acid; In 1,2-dichloro-ethane; at 80 ℃; for 3h;

DOI:10.1246/cl.1981.869

upstream raw materials:

1-(N-morpholino)cyclopent-1-ene

2-bromo-1-phenyl-ethanone oxime

Downstream raw materials:

4,5-dihydro-2-phenylcyclopentapyrrole

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