2-tert-butyl-2-(tri-tert-butylcyclopropenyl)-1,1,3,3,3-pentamethyl-1-phenyltrisilane

Base Information

Chemical Name:2-tert-butyl-2-(tri-tert-butylcyclopropenyl)-1,1,3,3,3-pentamethyl-1-phenyltrisilane
CAS No.:268561-17-7
Molecular Formula:C₃₀H₅₆Si₃
Molecular Weight:501.031
Hs Code.:

Synonyms:2-tert-butyl-2-(tri-tert-butylcyclopropenyl)-1,1,3,3,3-pentamethyl-1-phenyltrisilane

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Chemical Property of 2-tert-butyl-2-(tri-tert-butylcyclopropenyl)-1,1,3,3,3-pentamethyl-1-phenyltrisilane

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Technology Process of 2-tert-butyl-2-(tri-tert-butylcyclopropenyl)-1,1,3,3,3-pentamethyl-1-phenyltrisilane

There total 4 articles about 2-tert-butyl-2-(tri-tert-butylcyclopropenyl)-1,1,3,3,3-pentamethyl-1-phenyltrisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: tri-tert-butylcyclopropenylium tetrafluoroborate

: 268561-33-7
2-tert-butyl-2-chloro-1,1,3,3,3-pentamethyl-1-phenyltrisilane

: 268561-17-7
2-tert-butyl-2-(tri-tert-butylcyclopropenyl)-1,1,3,3,3-pentamethyl-1-phenyltrisilane

Guidance literature:: With lithium; In tetrahydrofuran; at -78 - 20 ℃; for 24h;
DOI:10.1002/1099-0690(200004)2000:7<1107::AID-EJOC1107>3.0.CO;2-8

Reference yield:

: 268561-29-1
1-bromo-1-tert-butyl-2,2,2-trimethyldisilane

: 268561-17-7
2-tert-butyl-2-(tri-tert-butylcyclopropenyl)-1,1,3,3,3-pentamethyl-1-phenyltrisilane

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / Li / tetrahydrofuran / 24 h / 20 °C

2: CCl₄ / 20 h / 50 °C

3: 47 percent / Li / tetrahydrofuran / 24 h / -78 - 20 °C

With tetrachloromethane; lithium; In tetrahydrofuran; 1: silylation / 2: Substitution / 3: Substitution;
DOI:10.1002/1099-0690(200004)2000:7<1107::AID-EJOC1107>3.0.CO;2-8

Reference yield:

: 268561-27-9
1-tert-butyl-2,2,2-trimethyl-1-phenyldisilane

: 268561-17-7
2-tert-butyl-2-(tri-tert-butylcyclopropenyl)-1,1,3,3,3-pentamethyl-1-phenyltrisilane

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / HBr / 48 h / -78 °C

2: 73 percent / Li / tetrahydrofuran / 24 h / 20 °C

3: CCl₄ / 20 h / 50 °C

4: 47 percent / Li / tetrahydrofuran / 24 h / -78 - 20 °C

With tetrachloromethane; hydrogen bromide; lithium; In tetrahydrofuran; 1: Substitution / 2: silylation / 3: Substitution / 4: Substitution;
DOI:10.1002/1099-0690(200004)2000:7<1107::AID-EJOC1107>3.0.CO;2-8