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C32H52O6Si

Base Information
  • Chemical Name:C32H52O6Si
  • CAS No.:1372122-83-2
  • Molecular Formula:C32H52O6Si
  • Molecular Weight:560.847
  • Hs Code.:
C<sub>32</sub>H<sub>52</sub>O<sub>6</sub>Si

Synonyms:C32H52O6Si

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Chemical Property of C32H52O6Si
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Technology Process of C32H52O6Si

There total 8 articles about C32H52O6Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With mercury(II) perchlorate tetrahydrate; water; calcium carbonate; In tetrahydrofuran; at 0 ℃; for 0.0125h;
DOI:10.1021/ol3007259
Guidance literature:
Multi-step reaction with 6 steps
1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 40 °C / Inert atmosphere
2.1: osmium(VIII) oxide; N,N,N,N,-tetramethylethylenediamine / dichloromethane / 14 h / -78 °C / Inert atmosphere
3.1: toluene-4-sulfonic acid / dichloromethane / 12 h / Inert atmosphere
4.1: tetrapropylammonium perruthenate; 4-methylmorpholine N-oxide / dichloromethane / 3 h / Inert atmosphere; Molecular sieve
5.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.67 h / -78 °C / Inert atmosphere
5.2: 2.5 h / -78 °C / Inert atmosphere
5.3: -78 °C / Inert atmosphere
6.1: mercury(II) perchlorate tetrahydrate; water; calcium carbonate / tetrahydrofuran / 0.01 h / 0 °C
With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; osmium(VIII) oxide; n-butyllithium; tetrapropylammonium perruthenate; mercury(II) perchlorate tetrahydrate; N,N,N,N,-tetramethylethylenediamine; water; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; calcium carbonate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1021/ol3007259
Guidance literature:
Multi-step reaction with 7 steps
1.1: methanol; lithium borohydride / diethyl ether / 0 - 20 °C
2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 40 °C / Inert atmosphere
3.1: osmium(VIII) oxide; N,N,N,N,-tetramethylethylenediamine / dichloromethane / 14 h / -78 °C / Inert atmosphere
4.1: toluene-4-sulfonic acid / dichloromethane / 12 h / Inert atmosphere
5.1: tetrapropylammonium perruthenate; 4-methylmorpholine N-oxide / dichloromethane / 3 h / Inert atmosphere; Molecular sieve
6.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.67 h / -78 °C / Inert atmosphere
6.2: 2.5 h / -78 °C / Inert atmosphere
6.3: -78 °C / Inert atmosphere
7.1: mercury(II) perchlorate tetrahydrate; water; calcium carbonate / tetrahydrofuran / 0.01 h / 0 °C
With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; methanol; osmium(VIII) oxide; lithium borohydride; n-butyllithium; tetrapropylammonium perruthenate; mercury(II) perchlorate tetrahydrate; N,N,N,N,-tetramethylethylenediamine; water; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; calcium carbonate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane;
DOI:10.1021/ol3007259
upstream raw materials:

C23H31NO2S2

C17H24O2

C15H20O2

C15H22O4

Downstream raw materials:

C18H20O5

C19H22O4

C21H26O4

C22H30O4

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