(2R)-1-(tert-Butoxycarbonyl)tetrahydro-1H-pyrrole-2-carboxylic 2-methylbutanoic anhydride

Base Information

• Chemical Name: (2R)-1-(tert-Butoxycarbonyl)tetrahydro-1H-pyrrole-2-carboxylic 2-methylbutanoic anhydride
• CAS No.: 1301760-11-1
• Molecular Formula: C₁₅H₂₅NO₅
• Molecular Weight: 299.367
• Mol file: 1301760-11-1.mol

Synonyms:C₁₅H₂₅NO₅

Chemical Property of (2R)-1-(tert-Butoxycarbonyl)tetrahydro-1H-pyrrole-2-carboxylic 2-methylbutanoic anhydride

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

(2R)-1-(tert-Butoxycarbonyl)tetrahydro-1H-pyrrole-2-carboxylic 2-methylbutanoic anhydride >95% ^*data from reagent suppliers

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Technology Process of (2R)-1-(tert-Butoxycarbonyl)tetrahydro-1H-pyrrole-2-carboxylic 2-methylbutanoic anhydride

There total 3 articles about (2R)-1-(tert-Butoxycarbonyl)tetrahydro-1H-pyrrole-2-carboxylic 2-methylbutanoic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → C15H25NO5 (1301760-11-1)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine

2: 4-methyl-morpholine

With 4-methyl-morpholine; triethylamine;

DOI:10.1016/j.ejmech.2011.05.010

Reference yield:

D-Prolin (344-25-2,25191-13-3,37159-97-0,4305-67-3,4607-28-7) → C15H25NO5 (1301760-11-1)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine

2: 4-methyl-morpholine

With 4-methyl-morpholine; triethylamine;

DOI:10.1016/j.ejmech.2011.05.010

Reference yield:

N-(tert-butoxycarbonyl)-D-proline (37784-17-1,59433-50-0) + isopentanoyl chloride (108-12-3) → C15H25NO5 (1301760-11-1)

Guidance literature:

With 4-methyl-morpholine;

DOI:10.1016/j.ejmech.2011.05.010

upstream raw materials:

di-tert-butyl dicarbonate

N-(tert-butoxycarbonyl)-D-proline

isopentanoyl chloride

D-Prolin

Downstream raw materials:

1-(tert-butoxycarbonyl)prolin-2R-ol

(R)-2-cyanomethyl pyrrolidine-1-carboxylic acid, tert-butyl ester

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