(3S)-3-(2-(benzyloxy)ethyl)-2-(3-methoxy-5-methylphenyl)-3-methylcyclopentanone

Base Information

• Chemical Name: (3S)-3-(2-(benzyloxy)ethyl)-2-(3-methoxy-5-methylphenyl)-3-methylcyclopentanone
• CAS No.: 1065253-15-7
• Molecular Formula: C₂₃H₂₈O₃
• Molecular Weight: 352.474

Synonyms:(3S)-3-(2-(benzyloxy)ethyl)-2-(3-methoxy-5-methylphenyl)-3-methylcyclopentanone

Chemical Property of (3S)-3-(2-(benzyloxy)ethyl)-2-(3-methoxy-5-methylphenyl)-3-methylcyclopentanone

Chemical Property:

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Technology Process of (3S)-3-(2-(benzyloxy)ethyl)-2-(3-methoxy-5-methylphenyl)-3-methylcyclopentanone

There total 1 articles about (3S)-3-(2-(benzyloxy)ethyl)-2-(3-methoxy-5-methylphenyl)-3-methylcyclopentanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

(5R)-7-(benzyloxy)-1-(3-methoxy-5-methylphenyl)-5-methyl-1-diazoheptan-2-one (1065253-12-4) → (3S)-3-(2-(benzyloxy)ethyl)-2-(3-methoxy-5-methylphenyl)-3-methylcyclopentanone (1065253-15-7)

Guidance literature:

dirhodium(II) tetrakis[N-phthaloyl-(S)-t-leucinate]; In toluene; at 20 ℃; for 0.25h;

DOI:10.1021/jo8010683

Reference yield: 98.0%

(3S)-3-(2-(benzyloxy)ethyl)-2-(3-methoxy-5-methylphenyl)-3-methylcyclopentanone (1065253-15-7) → (3S)-3-(2-hydroxyethyl)-2-(3-methoxy-5-methylphenyl)-3-methylcyclopentanone (1065253-26-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1021/jo8010683

upstream raw materials:

(5R)-7-(benzyloxy)-1-(3-methoxy-5-methylphenyl)-5-methyl-1-diazoheptan-2-one

Downstream raw materials:

(3S)-3-(2-hydroxyethyl)-2-(3-methoxy-5-methylphenyl)-3-methylcyclopentanone

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