methyl 4-[2-(8,8-dimethyl-5,6,7,8-tetrahydronaphthalen-2-yl)allyloxy]-3-iodobenzoate

Base Information

Chemical Name:methyl 4-[2-(8,8-dimethyl-5,6,7,8-tetrahydronaphthalen-2-yl)allyloxy]-3-iodobenzoate
CAS No.:207865-37-0
Molecular Formula:C₂₃H₂₅IO₃
Molecular Weight:476.354
Hs Code.:

Synonyms:methyl 4-[2-(8,8-dimethyl-5,6,7,8-tetrahydronaphthalen-2-yl)allyloxy]-3-iodobenzoate

Suppliers and Price of methyl 4-[2-(8,8-dimethyl-5,6,7,8-tetrahydronaphthalen-2-yl)allyloxy]-3-iodobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 4-[2-(8,8-dimethyl-5,6,7,8-tetrahydronaphthalen-2-yl)allyloxy]-3-iodobenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 4-[2-(8,8-dimethyl-5,6,7,8-tetrahydronaphthalen-2-yl)allyloxy]-3-iodobenzoate

There total 3 articles about methyl 4-[2-(8,8-dimethyl-5,6,7,8-tetrahydronaphthalen-2-yl)allyloxy]-3-iodobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 207865-34-7
methyl 4-[2-(8,8-dimethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-2-oxoethoxy]-3-iodobenzoate

: 207865-37-0
methyl 4-[2-(8,8-dimethyl-5,6,7,8-tetrahydronaphthalen-2-yl)allyloxy]-3-iodobenzoate

Guidance literature:

Reference yield:

: 15126-06-4
methyl 3-iodo-4-hydroxybenzoate

: 207865-37-0
methyl 4-[2-(8,8-dimethyl-5,6,7,8-tetrahydronaphthalen-2-yl)allyloxy]-3-iodobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / K₂CO₃ / butan-2-one / 4 h / Heating

2: 59 percent / NaOCH₃ / methanol; tetrahydrofuran / 12 h / Ambient temperature

With sodium methylate; potassium carbonate; In tetrahydrofuran; methanol; butanone;
DOI:10.1016/S0040-4020(98)00169-0

Reference yield:

: 2-Bromo-1-(8,8-dimethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)-ethanone

: 207865-37-0
methyl 4-[2-(8,8-dimethyl-5,6,7,8-tetrahydronaphthalen-2-yl)allyloxy]-3-iodobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / K₂CO₃ / butan-2-one / 4 h / Heating

2: 59 percent / NaOCH₃ / methanol; tetrahydrofuran / 12 h / Ambient temperature

With sodium methylate; potassium carbonate; In tetrahydrofuran; methanol; butanone;
DOI:10.1016/S0040-4020(98)00169-0