(2E,4E,6E,8E,10E,12E,14E)-4,9,13-trimethyl-15-(2,6,6-trimethylcyclohex-1-en-1-yl)pentadeca-2,4,6,8,10,12,14-heptaen-1-ol

Base Information

Chemical Name:(2E,4E,6E,8E,10E,12E,14E)-4,9,13-trimethyl-15-(2,6,6-trimethylcyclohex-1-en-1-yl)pentadeca-2,4,6,8,10,12,14-heptaen-1-ol
CAS No.:6541-42-0
Molecular Formula:C₂₇H₃₈O
Molecular Weight:378.598
Hs Code.:

Synonyms:(2E,4E,6E,8E,10E,12E,14E)-4,9,13-trimethyl-15-(2,6,6-trimethylcyclohex-1-en-1-yl)pentadeca-2,4,6,8,10,12,14-heptaen-1-ol

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Chemical Property of (2E,4E,6E,8E,10E,12E,14E)-4,9,13-trimethyl-15-(2,6,6-trimethylcyclohex-1-en-1-yl)pentadeca-2,4,6,8,10,12,14-heptaen-1-ol

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Technology Process of (2E,4E,6E,8E,10E,12E,14E)-4,9,13-trimethyl-15-(2,6,6-trimethylcyclohex-1-en-1-yl)pentadeca-2,4,6,8,10,12,14-heptaen-1-ol

There total 7 articles about (2E,4E,6E,8E,10E,12E,14E)-4,9,13-trimethyl-15-(2,6,6-trimethylcyclohex-1-en-1-yl)pentadeca-2,4,6,8,10,12,14-heptaen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 432552-01-7
4,9,13-trimethyl-15-(2,6,6-trimethylcyclohex-1-enyl)pentadeca-2,4,6,8,10,12,14-heptanoic acid ethyl ester

: 6541-42-0
(2E,4E,6E,8E,10E,12E,14E)-4,9,13-trimethyl-15-(2,6,6-trimethylcyclohex-1-en-1-yl)pentadeca-2,4,6,8,10,12,14-heptaen-1-ol

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; cyclohexane; at 0 ℃; for 0.5h;
DOI:10.1002/jlcr.536

Reference yield:

: 69774-12-5
methyl (2E,4E,6E,8E,10E,12E,14E)-4,9,13-trimethyl-15-(2,6,6-trimethylcyclohex-1-en-1-yl)pentadeca-2,4,6,8,10,12,14-heptaenoate

: 6541-42-0
(2E,4E,6E,8E,10E,12E,14E)-4,9,13-trimethyl-15-(2,6,6-trimethylcyclohex-1-en-1-yl)pentadeca-2,4,6,8,10,12,14-heptaen-1-ol

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at -78 ℃; for 2h;
DOI:10.1016/j.tet.2018.03.050

Reference yield:

: 5056-17-7
(2E,4E,6E)-2,7-dimethyl-2,4,6-octatrienedial

: 6541-42-0
(2E,4E,6E,8E,10E,12E,14E)-4,9,13-trimethyl-15-(2,6,6-trimethylcyclohex-1-en-1-yl)pentadeca-2,4,6,8,10,12,14-heptaen-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methoxide / methanol / 0.5 h / 0 °C

2: 71 percent / tetrahydrofuran / 5 h / 95 °C

3: 99 percent / DIBAL / diethyl ether; cyclohexane / 0.5 h / 0 °C

With sodium methylate; diisobutylaluminium hydride; In tetrahydrofuran; methanol; diethyl ether; cyclohexane; 1: Wittig olefination / 2: Wittig reaction;
DOI:10.1002/jlcr.536