N₂-[1-(N-carbamoyl-S-methylsulfinimidoyl)-2-methylpropan-2-yl]-3-iodo-N₁-[3-(trifluoromethyl)phenyl]phthalamide

Base Information

• Chemical Name: N₂-[1-(N-carbamoyl-S-methylsulfinimidoyl)-2-methylpropan-2-yl]-3-iodo-N₁-[3-(trifluoromethyl)phenyl]phthalamide
• CAS No.: 1634718-47-0
• Molecular Formula: C₂₁H₂₂F₃IN₄O₃S
• Molecular Weight: 594.396

Synonyms:N₂-[1-(N-carbamoyl-S-methylsulfinimidoyl)-2-methylpropan-2-yl]-3-iodo-N₁-[3-(trifluoromethyl)phenyl]phthalamide

Chemical Property of N₂-[1-(N-carbamoyl-S-methylsulfinimidoyl)-2-methylpropan-2-yl]-3-iodo-N₁-[3-(trifluoromethyl)phenyl]phthalamide

Chemical Property:

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Technology Process of N₂-[1-(N-carbamoyl-S-methylsulfinimidoyl)-2-methylpropan-2-yl]-3-iodo-N₁-[3-(trifluoromethyl)phenyl]phthalamide

There total 2 articles about N₂-[1-(N-carbamoyl-S-methylsulfinimidoyl)-2-methylpropan-2-yl]-3-iodo-N₁-[3-(trifluoromethyl)phenyl]phthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.3%

N2-(1-(N-cyano-S-methylsulfinimidoyl)-2-methylpropan-2-yl)-3-iodo-N1-(3-(trifluoromethyl)phenyl)phthalamide (1383473-51-5) → N2-[1-(N-carbamoyl-S-methylsulfinimidoyl)-2-methylpropan-2-yl]-3-iodo-N1-[3-(trifluoromethyl)phenyl]phthalamide (1634718-47-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1002/cjoc.201400223

Reference yield:

N2-[1,1-dimethyl-2-(methylthio)ethyl]-3-iodo-N1-[3-(trifluoromethyl)phenyl]-1,2-benzenedicarboxamide (1253787-08-4) → N2-[1-(N-carbamoyl-S-methylsulfinimidoyl)-2-methylpropan-2-yl]-3-iodo-N1-[3-(trifluoromethyl)phenyl]phthalamide (1634718-47-0)

Guidance literature:

Multi-step reaction with 2 steps

1: [bis(acetoxy)iodo]benzene / acetonitrile / 1.5 h / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C

With [bis(acetoxy)iodo]benzene; trifluoroacetic acid; In dichloromethane; acetonitrile;

DOI:10.1002/cjoc.201400223

Reference yield: 86.8%

N2-[1-(N-carbamoyl-S-methylsulfinimidoyl)-2-methylpropan-2-yl]-3-iodo-N1-[3-(trifluoromethyl)phenyl]phthalamide (1634718-47-0) → N2-(1-(N-carbamoyl-S-methylsulfonimidoyl)-2-methylpropan-2-yl)-3-iodo-N1-(3-(trifluoromethyl)phenyl)phthalamide (1634718-39-0)

Guidance literature:

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In ethanol; at 0 - 20 ℃; for 1.25h;

DOI:10.1002/cjoc.201400223

upstream raw materials:

N₂-[1,1-dimethyl-2-(methylthio)ethyl]-3-iodo-N₁-[3-(trifluoromethyl)phenyl]-1,2-benzenedicarboxamide

N₂-(1-(N-cyano-S-methylsulfinimidoyl)-2-methylpropan-2-yl)-3-iodo-N₁-(3-(trifluoromethyl)phenyl)phthalamide

Downstream raw materials:

N₂-(1-(N-carbamoyl-S-methylsulfonimidoyl)-2-methylpropan-2-yl)-3-iodo-N₁-(3-(trifluoromethyl)phenyl)phthalamide

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