Technology Process of C52H52N2O13S2
There total 7 articles about C52H52N2O13S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
tetrahydrofuran;
for 48h;
Inert atmosphere;
Reflux;
DOI:10.1016/j.tet.2010.12.006
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / Cooling with acetone-dry ice; Inert atmosphere
1.2: 1 h / -78 °C / Inert atmosphere
2.1: oxalyl dichloride / benzene / Reflux
3.1: sodium hydride / tetrahydrofuran / 48 h / Inert atmosphere; Reflux
With
n-butyllithium; oxalyl dichloride; sodium hydride;
In
tetrahydrofuran; hexane; benzene;
DOI:10.1016/j.tet.2010.12.006
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate / acetonitrile / Reflux
2.1: bromine / chloroform / 4 h / 0 - 20 °C
3.1: caesium carbonate / acetonitrile / 0.5 h / Reflux; Inert atmosphere
3.2: 67 h / Reflux; Inert atmosphere
4.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / Cooling with acetone-dry ice; Inert atmosphere
4.2: 1 h / -78 °C / Inert atmosphere
5.1: oxalyl dichloride / benzene / Reflux
6.1: sodium hydride / tetrahydrofuran / 48 h / Inert atmosphere; Reflux
With
n-butyllithium; oxalyl dichloride; bromine; sodium hydride; potassium carbonate; caesium carbonate;
In
tetrahydrofuran; hexane; chloroform; acetonitrile; benzene;
DOI:10.1016/j.tet.2010.12.006
