N⁶-4-monomethoxytrityl-9-{2-[(3-methyl-cycloSal)phosphonylmethoxy]ethyl}adenine

Base Information

Chemical Name:N⁶-4-monomethoxytrityl-9-{2-[(3-methyl-cycloSal)phosphonylmethoxy]ethyl}adenine
CAS No.:872191-08-7
Molecular Formula:C₃₆H₃₄N₅O₅P
Molecular Weight:647.67
Hs Code.:

N<sup>6</sup>-4-monomethoxytrityl-9-{2-[(3-methyl-cycloSal)phosphonylmethoxy]ethyl}adenine

Synonyms:N⁶-4-monomethoxytrityl-9-{2-[(3-methyl-cycloSal)phosphonylmethoxy]ethyl}adenine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁶-4-monomethoxytrityl-9-{2-[(3-methyl-cycloSal)phosphonylmethoxy]ethyl}adenine

Chemical Property:

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Technology Process of N⁶-4-monomethoxytrityl-9-{2-[(3-methyl-cycloSal)phosphonylmethoxy]ethyl}adenine

There total 5 articles about N⁶-4-monomethoxytrityl-9-{2-[(3-methyl-cycloSal)phosphonylmethoxy]ethyl}adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₂₆Cl₂N₅O₃P

: 22470-99-1
3-methylsalicyl alcohol

: 872191-08-7
N⁶-4-monomethoxytrityl-9-{2-[(3-methyl-cycloSal)phosphonylmethoxy]ethyl}adenine

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jm050641a

Reference yield:

: 153235-85-9
N⁶-4-monomethoxytrityl-9-[2-(diethylphosphonylmethoxy)ethyl]adenine

: 872191-08-7
N⁶-4-monomethoxytrityl-9-{2-[(3-methyl-cycloSal)phosphonylmethoxy]ethyl}adenine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / acetonitrile / 16 h / 20 °C

2: PCl₅ / CH₂Cl₂ / 2.5 h / 20 °C

3: 102 mg / Et₃N / CH₂Cl₂ / 0 - 20 °C

With pyridine; phosphorus pentachloride; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/jm050641a

Reference yield:

: C₃₄H₄₄N₅O₅PSi₂

: 872191-08-7
N⁶-4-monomethoxytrityl-9-{2-[(3-methyl-cycloSal)phosphonylmethoxy]ethyl}adenine

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₅ / CH₂Cl₂ / 2.5 h / 20 °C

2: 102 mg / Et₃N / CH₂Cl₂ / 0 - 20 °C

With phosphorus pentachloride; triethylamine; In dichloromethane;
DOI:10.1021/jm050641a