[(4-benzyloxy-benzenesulfonyl)-(4-oxo-pentyl)-amino]-acetic acid tert-butyl ester

Base Information

• Chemical Name: [(4-benzyloxy-benzenesulfonyl)-(4-oxo-pentyl)-amino]-acetic acid tert-butyl ester
• CAS No.: 329041-21-6
• Molecular Formula: C₂₄H₃₁NO₆S
• Molecular Weight: 461.579

Synonyms:[(4-benzyloxy-benzenesulfonyl)-(4-oxo-pentyl)-amino]-acetic acid tert-butyl ester

Chemical Property of [(4-benzyloxy-benzenesulfonyl)-(4-oxo-pentyl)-amino]-acetic acid tert-butyl ester

Chemical Property:

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Technology Process of [(4-benzyloxy-benzenesulfonyl)-(4-oxo-pentyl)-amino]-acetic acid tert-butyl ester

There total 5 articles about [(4-benzyloxy-benzenesulfonyl)-(4-oxo-pentyl)-amino]-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[(4-benzyloxy-benzenesulfonyl)-pent-4-enyl-amino]-acetic acid tert-butyl ester (329041-20-5) → [(4-benzyloxy-benzenesulfonyl)-(4-oxo-pentyl)-amino]-acetic acid tert-butyl ester (329041-21-6)

Guidance literature:

With oxygen; copper(l) chloride; palladium dichloride; In DMF (N,N-dimethyl-formamide); water; for 72h;

Reference yield:

[(4-benzyloxy-benzenesulfonyl)-pent-4-enyl-amino]-acetic acid tert-butyl ester (329041-20-5) + palladium dichloride → [(4-benzyloxy-benzenesulfonyl)-(4-oxo-pentyl)-amino]-acetic acid tert-butyl ester (329041-21-6)

Guidance literature:

copper(I) chloride; In N-methyl-acetamide; water;

Reference yield:

[4-benzyloxybenzenesulfonylamino]-acetic acid tert-butyl ester (329041-19-2) + 5-Hydroxy-2-pentanone (1071-73-4) → [(4-benzyloxy-benzenesulfonyl)-(4-oxo-pentyl)-amino]-acetic acid tert-butyl ester (329041-21-6)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 23 ℃;

DOI:10.1016/j.bmcl.2005.05.037

upstream raw materials:

[4-benzyloxybenzenesulfonylamino]-acetic acid tert-butyl ester

5-Hydroxy-2-pentanone

Glycine tert-butyl ester

p-benzyloxybenzenesulfonyl chloride

Downstream raw materials:

(2R,3R)-1-(4-Benzyloxy-benzenesulfonyl)-3-hydroxy-3-methyl-piperidine-2-carboxylic acid tert-butyl ester

(2R,3S)-1-(4-Benzyloxy-benzenesulfonyl)-3-hydroxy-3-methyl-piperidine-2-carboxylic acid tert-butyl ester

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