1-(2-methyl-5-(4-hexadecylcarbamoylphenyl)thiophene-3-yl)-2-(2-methyl-5-(4-dodecanoxyphenyl)thiophene-3-yl)hexafluorocyclopentene

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Chemical Name:1-(2-methyl-5-(4-hexadecylcarbamoylphenyl)thiophene-3-yl)-2-(2-methyl-5-(4-dodecanoxyphenyl)thiophene-3-yl)hexafluorocyclopentene
CAS No.:1628293-16-2
Molecular Formula:C₅₆H₇₅F₆NO₂S₂
Molecular Weight:972.339
Hs Code.:

Synonyms:1-(2-methyl-5-(4-hexadecylcarbamoylphenyl)thiophene-3-yl)-2-(2-methyl-5-(4-dodecanoxyphenyl)thiophene-3-yl)hexafluorocyclopentene

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Chemical Property of 1-(2-methyl-5-(4-hexadecylcarbamoylphenyl)thiophene-3-yl)-2-(2-methyl-5-(4-dodecanoxyphenyl)thiophene-3-yl)hexafluorocyclopentene

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Technology Process of 1-(2-methyl-5-(4-hexadecylcarbamoylphenyl)thiophene-3-yl)-2-(2-methyl-5-(4-dodecanoxyphenyl)thiophene-3-yl)hexafluorocyclopentene

There total 2 articles about 1-(2-methyl-5-(4-hexadecylcarbamoylphenyl)thiophene-3-yl)-2-(2-methyl-5-(4-dodecanoxyphenyl)thiophene-3-yl)hexafluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: N-hexadecyl-4-iodobenzamide

: 116223-59-7
1-(dodecyloxy)-4-iodobenzene

: 3-(3,3,4,4,5,5-hexafluoro-2-(5-iodo-2-methylthiophen-3-yl)cyclopent-1-enyl)-5-iodo-2-methylthiophene

: 1628293-15-1
1,2-bis(2-methyl-5-(4-hexadecylcarbamoylphenyl)thiophene-3-yl)hexafluorocyclopentene

: 1628293-16-2
1-(2-methyl-5-(4-hexadecylcarbamoylphenyl)thiophene-3-yl)-2-(2-methyl-5-(4-dodecanoxyphenyl)thiophene-3-yl)hexafluorocyclopentene

: 1628293-17-3
1,2-bis(2-methyl-5-(4-dodecanoxyphenyl)thiophene-3-yl)hexafluorocyclopentene

Guidance literature:: 3-(3,3,4,4,5,5-hexafluoro-2-(5-iodo-2-methylthiophen-3-yl)cyclopent-1-enyl)-5-iodo-2-methylthiophene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

With boric acid tributyl ester; In tetrahydrofuran; for 1h; Inert atmosphere;

N-hexadecyl-4-iodobenzamide; 1-(dodecyloxy)-4-iodobenzene; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; for 2h; Inert atmosphere; Reflux;
DOI:10.1246/cl.130705