dimesityldioxo-osmium(VI)

Base Information

Chemical Name:dimesityldioxo-osmium(VI)
CAS No.:110781-72-1
Molecular Formula:C₁₈H₂₂O₂Os
Molecular Weight:460.571
Hs Code.:

Synonyms:dimesityldioxo-osmium(VI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimesityldioxo-osmium(VI)

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Technology Process of dimesityldioxo-osmium(VI)

There total 1 articles about dimesityldioxo-osmium(VI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 20816-12-0
osmium(VIII) oxide

: 2633-66-1
2-mesitylmagnesium bromide

: 110781-72-1
dimesityldioxo-osmium(VI)

Guidance literature:: With O₂; In tetrahydrofuran; diethyl ether; under Ar, to stirred soln. of OsO4 in THF at -78°C added Me3C6H2MgBr (0.93 M soln. in Et2O), allowed to warm slowly to room temp. and stirred for ca. 1 h, evapd. in vac., O2 satd. petroleum added, stirred overnight; filtrate concd., cooled to -20°C; elem. anal.;

Reference yield: 96.0%

: 110781-72-1
dimesityldioxo-osmium(VI)

: trans-(2,2'-bipyridyl)dimesityldioxo-osmium(VI)

Guidance literature:: With (C₅H₄N)2; In diethyl ether; addn. of bipyridyl to a soln. of OsO2(mes)2 in Et2O gives an orange ppt., stirring at room temp. for 2 h (under exclusion of air); removal of the solvent in vacuo, extn. into warm Et2O which is concentrated and cooled to -20°C, elem. anal.;

Reference yield: 96.0%

: 110781-72-1
dimesityldioxo-osmium(VI)

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: cis-(2,6-dimethylphenyl isocyanide)dimesityldioxo-osmium(VI)

Guidance literature:: In hexane; addn. of isocyanide to a soln. of OsO2(mes)2 in hexane (under exclusion of air); collection, crystn. from Et2O, elem. anal.;