(Z)-1-methoxy-4-phenylsulfonyl-6-phenylhex-3-en-5-yne

Base Information

Chemical Name:(Z)-1-methoxy-4-phenylsulfonyl-6-phenylhex-3-en-5-yne
CAS No.:1581883-45-5
Molecular Formula:C₁₉H₁₈O₃S
Molecular Weight:326.416
Hs Code.:

Synonyms:(Z)-1-methoxy-4-phenylsulfonyl-6-phenylhex-3-en-5-yne

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Chemical Property of (Z)-1-methoxy-4-phenylsulfonyl-6-phenylhex-3-en-5-yne

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Technology Process of (Z)-1-methoxy-4-phenylsulfonyl-6-phenylhex-3-en-5-yne

There total 2 articles about (Z)-1-methoxy-4-phenylsulfonyl-6-phenylhex-3-en-5-yne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: C₂₃H₄₀O₃SSn

: 932-87-6
1-Bromo-2-phenylacetylene

: 1581883-45-5
(Z)-1-methoxy-4-phenylsulfonyl-6-phenylhex-3-en-5-yne

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; at 20 ℃; Inert atmosphere;
DOI:10.3184/174751913X13816588007726

Reference yield:

: 1372674-57-1
C₁₁H₁₂O₃S

: 1581883-45-5
(Z)-1-methoxy-4-phenylsulfonyl-6-phenylhex-3-en-5-yne

Guidance literature:: Multi-step reaction with 2 steps

1: Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / 1,2-dimethoxyethane / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; 2: |Stille Cross Coupling;
DOI:10.3184/174751913X13816588007726

Reference yield: 81.0%

: 1581883-45-5
(Z)-1-methoxy-4-phenylsulfonyl-6-phenylhex-3-en-5-yne

: 688-73-3
tri-n-butyl-tin hydride

: (1E,3Z)-1-phenyl-2-tributylstannyl-3-phenylsulfonyl-6-methoxyhexa-1,3-diene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 4h; stereoselective reaction; Inert atmosphere;
DOI:10.3184/174751913X13816588007726