4-Benzyl 1-t-Butyl N-t-Butyloxycarbonyl-N-ethoxycarbonylmethyl-L-aspartate

Base Information

Chemical Name:4-Benzyl 1-t-Butyl N-t-Butyloxycarbonyl-N-ethoxycarbonylmethyl-L-aspartate
CAS No.:125989-84-6
Molecular Formula:C₂₄H₃₅NO₈
Molecular Weight:465.544
Hs Code.:

Synonyms:4-Benzyl 1-t-Butyl N-t-Butyloxycarbonyl-N-ethoxycarbonylmethyl-L-aspartate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Benzyl 1-t-Butyl N-t-Butyloxycarbonyl-N-ethoxycarbonylmethyl-L-aspartate

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Technology Process of 4-Benzyl 1-t-Butyl N-t-Butyloxycarbonyl-N-ethoxycarbonylmethyl-L-aspartate

There total 2 articles about 4-Benzyl 1-t-Butyl N-t-Butyloxycarbonyl-N-ethoxycarbonylmethyl-L-aspartate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 125989-83-5
4-Benzyl 1-t-Butyl N-Ethoxycarbonylmethyl-L-aspartate

: 125989-84-6
4-Benzyl 1-t-Butyl N-t-Butyloxycarbonyl-N-ethoxycarbonylmethyl-L-aspartate

Guidance literature:: With triethylamine; In 1,4-dioxane; water; at 50 ℃; for 8h;
DOI:10.1002/jhet.5570260322

Reference yield:

: 94347-11-2
4-benzyl 1-t-butyl L-aspartate

: 125989-84-6
4-Benzyl 1-t-Butyl N-t-Butyloxycarbonyl-N-ethoxycarbonylmethyl-L-aspartate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / triethylamine / dimethylformamide / 0.5 h / Ambient temperature

2: 96 percent / triethylamine / dioxane; H₂O / 8 h / 50 °C

With triethylamine; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570260322