N^ε-Fmoc-Lys benzyl eater p-toluenesulfonate

Base Information

Chemical Name:N^ε-Fmoc-Lys benzyl eater p-toluenesulfonate
CAS No.:84624-14-6
Molecular Formula:C₇H₈O₃S*C₂₈H₃₀N₂O₄
Molecular Weight:630.762
Hs Code.:

N<sup>ε</sup>-Fmoc-Lys benzyl eater p-toluenesulfonate

Synonyms:N^ε-Fmoc-Lys benzyl eater p-toluenesulfonate

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Chemical Property of N^ε-Fmoc-Lys benzyl eater p-toluenesulfonate

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Technology Process of N^ε-Fmoc-Lys benzyl eater p-toluenesulfonate

There total 2 articles about N^ε-Fmoc-Lys benzyl eater p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 104-15-4
toluene-4-sulfonic acid

: 84624-29-3
N^ε-Fmoc-Lys trifluoroacetate

: 100-51-6,185532-71-2
benzyl alcohol

: 84624-14-6
N^ε-Fmoc-Lys benzyl eater p-toluenesulfonate

Guidance literature:: In benzene; for 24h; Heating;
DOI:10.1021/jm00359a004

Reference yield:

: 84624-27-1
Boc-Lys(Fmoc)-OH

: 84624-14-6
N^ε-Fmoc-Lys benzyl eater p-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 3.35 g / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 78 percent / benzene / 24 h / Heating

In dichloromethane; benzene;
DOI:10.1021/jm00359a004

Reference yield: 68.0%

: 13139-15-6,53296-34-7
N-tert-butoxycarbonyl-L-leucine

: 84624-14-6
N^ε-Fmoc-Lys benzyl eater p-toluenesulfonate

: 84624-15-7
Boc-Leu-Lys(Fmoc) benzyl ester

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 0 - 25 ℃; for 17h;
DOI:10.1021/jm00359a004