triphenylgermane-d₁

Base Information

Chemical Name:triphenylgermane-d₁
CAS No.:2816-42-4
Molecular Formula:C₁₈H₁₆Ge
Molecular Weight:305.907
Hs Code.:

Synonyms:triphenylgermane-d₁

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylgermane-d₁

Chemical Property:

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Technology Process of triphenylgermane-d₁

There total 8 articles about triphenylgermane-d₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 2816-43-5
triphenylgermane

: 2816-42-4
triphenylgermane-d₁

Guidance literature:: With RhH{κ³-P,O,P-[9,9-dimethyl-4,5-bis-(diisopropylphosphino)xanthene₂]}; deuterium; In diethyl ether; at 25 ℃; for 6h; under 855.086 Torr; Inert atmosphere; Glovebox; Schlenk technique;
DOI:10.1021/acs.joc.0c01967

Reference yield: 53.0%

: CH₃(C₆H₅)((C₆H₅)3Ge)SiOCH₃

: 2816-42-4
triphenylgermane-d₁

: 86962-19-8
CH₃(C₆H₅)((C₆H₅)3Ge)Si⁽²⁾H

: 2816-43-5
triphenylgermane

Guidance literature:: With lithium aluminium deuteride; In diethyl ether; byproducts: MePhSiD2; to LiAlH4 in ether was added equimolar amt. of silane, room temp., 24 h, N2 atm.; hydrolysis with D2O, extn. (ether), evapn.;
DOI:10.1016/S0022-328X(00)98847-8

Reference yield: 50.0%

: CH₃(C₆H₅)((C₆H₅)3Ge)SiH

: 2816-42-4
triphenylgermane-d₁

: 2816-43-5
triphenylgermane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; byproducts: MePhSiH2, MePhSiHD, MePhSiD2; to LiAlH4 in ether was added equimolar amt. of silane, room temp., 48 h, N2 atm.; hydrolysis with D2O, extn. (ether), evapn.;
DOI:10.1016/S0022-328X(00)98847-8