2-(4-amino-phenyl)-1H-benzoimidazole-5-carboxylic acid adamantan-1-ylamide

Base Information

Chemical Name:2-(4-amino-phenyl)-1H-benzoimidazole-5-carboxylic acid adamantan-1-ylamide
CAS No.:820242-66-8
Molecular Formula:C₂₄H₂₆N₄O
Molecular Weight:386.497
Hs Code.:

2-(4-amino-phenyl)-1<i>H</i>-benzoimidazole-5-carboxylic acid adamantan-1-ylamide

Synonyms:2-(4-amino-phenyl)-1H-benzoimidazole-5-carboxylic acid adamantan-1-ylamide

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Chemical Property of 2-(4-amino-phenyl)-1H-benzoimidazole-5-carboxylic acid adamantan-1-ylamide

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Technology Process of 2-(4-amino-phenyl)-1H-benzoimidazole-5-carboxylic acid adamantan-1-ylamide

There total 4 articles about 2-(4-amino-phenyl)-1H-benzoimidazole-5-carboxylic acid adamantan-1-ylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 820242-64-6
2-(4-nitro-phenyl)-1H-benzoimidazole-5-carboxylic acid adamantan-1-ylamide

: 820242-66-8
2-(4-amino-phenyl)-1H-benzoimidazole-5-carboxylic acid adamantan-1-ylamide

Guidance literature:: With N,N-dimethyl-formamide; palladium on activated charcoal; In methanol;
DOI:10.1021/jm049288j

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 820242-66-8
2-(4-amino-phenyl)-1H-benzoimidazole-5-carboxylic acid adamantan-1-ylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 55 percent / nitrobenzene / 18 h / 155 - 160 °C

2.1: 1,1'-carbonyldiimidazole / dimethylformamide / 3 h / 80 °C

2.2: dimethylformamide / 18 h / Heating

3.1: H₂ / Pd/C / ethanol; dimethylformamide / 6 h / 70 - 90 °C

With hydrogen; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In ethanol; nitrobenzene; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2006.03.014

Reference yield:

: 69570-99-6
2-(4-nitrophenyl)-1H-benzimidazole-5-carboxylic acid

: 820242-66-8
2-(4-amino-phenyl)-1H-benzoimidazole-5-carboxylic acid adamantan-1-ylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,1'-carbonyldiimidazole / dimethylformamide / 3 h / 80 °C

1.2: dimethylformamide / 18 h / Heating

2.1: H₂ / Pd/C / ethanol; dimethylformamide / 6 h / 70 - 90 °C

With hydrogen; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2006.03.014