C₁₇H₂₄O₅

Base Information

Chemical Name:C₁₇H₂₄O₅
CAS No.:1592771-59-9
Molecular Formula:C₁₇H₂₄O₅
Molecular Weight:308.375
Hs Code.:

C<sub>17</sub>H<sub>24</sub>O<sub>5</sub>

Synonyms:C₁₇H₂₄O₅

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Chemical Property of C₁₇H₂₄O₅

Chemical Property:

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Technology Process of C₁₇H₂₄O₅

There total 10 articles about C₁₇H₂₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1592771-58-8
C₁₇H₂₂O₅

: 1592771-59-9
C₁₇H₂₄O₅

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at -80 ℃; for 0.5h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol500788c

Reference yield:

: methyl 3-O-benzyl-5-O-(p-toluenesulfonyl)-2-deoxy-D-ribofuranoside

: 1592771-59-9
C₁₇H₂₄O₅

Guidance literature:: Multi-step reaction with 7 steps

1: lithium triethylborohydride / tetrahydrofuran / 6.25 h / 20 - 45 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 0.67 h / 0 - 20 °C / Inert atmosphere

3: 4-methyl-morpholine / dichloromethane / 2 h / 20 °C / Inert atmosphere

4: methyl iodide; sodium hydrogencarbonate / acetonitrile; water / 24 h / 20 °C

5: samarium diiodide / acetonitrile; methanol / 1 h / -20 °C / Inert atmosphere

6: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

7: sodium tetrahydroborate / dichloromethane; methanol / 0.5 h / -80 °C / Inert atmosphere

With 4-methyl-morpholine; sodium tetrahydroborate; samarium diiodide; boron trifluoride diethyl etherate; lithium triethylborohydride; sodium hydrogencarbonate; Dess-Martin periodane; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; 6: |Dess-Martin Oxidation;
DOI:10.1021/ol500788c

Reference yield:

: methyl 3-O-benzyl-2,5-dideoxy-D-erythropentofuranoside

: 1592771-59-9
C₁₇H₂₄O₅

Guidance literature:: Multi-step reaction with 6 steps

1: boron trifluoride diethyl etherate / dichloromethane / 0.67 h / 0 - 20 °C / Inert atmosphere

2: 4-methyl-morpholine / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: methyl iodide; sodium hydrogencarbonate / acetonitrile; water / 24 h / 20 °C

4: samarium diiodide / acetonitrile; methanol / 1 h / -20 °C / Inert atmosphere

5: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

6: sodium tetrahydroborate / dichloromethane; methanol / 0.5 h / -80 °C / Inert atmosphere

With 4-methyl-morpholine; sodium tetrahydroborate; samarium diiodide; boron trifluoride diethyl etherate; sodium hydrogencarbonate; Dess-Martin periodane; methyl iodide; In methanol; dichloromethane; water; acetonitrile; 5: |Dess-Martin Oxidation;
DOI:10.1021/ol500788c