4-[(4-(3,6-di-tert-butyl-9H-carbazol-9-yl)phenoxy)methyl]benzaldehyde

Base Information

• Chemical Name: 4-[(4-(3,6-di-tert-butyl-9H-carbazol-9-yl)phenoxy)methyl]benzaldehyde
• CAS No.: 1620641-13-5
• Molecular Formula: C₃₄H₃₅NO₂
• Molecular Weight: 489.657
• Mol file: 1620641-13-5.mol

Synonyms:4-[(4-(3,6-di-tert-butyl-9H-carbazol-9-yl)phenoxy)methyl]benzaldehyde

Chemical Property of 4-[(4-(3,6-di-tert-butyl-9H-carbazol-9-yl)phenoxy)methyl]benzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 4-[(4-(3,6-di-tert-butyl-9H-carbazol-9-yl)phenoxy)methyl]benzaldehyde

There total 1 articles about 4-[(4-(3,6-di-tert-butyl-9H-carbazol-9-yl)phenoxy)methyl]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

4-(3,6-di-tert-butyl-9H-carbazol-9-yl)phenol (929874-30-6) + 4-(bromomethyl)benzaldehyde (51359-78-5) → 4-[(4-(3,6-di-tert-butyl-9H-carbazol-9-yl)phenoxy)methyl]benzaldehyde (1620641-13-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; Inert atmosphere;

DOI:10.1039/c3ra45660a

Reference yield: 34.0%

4-[(4-(3,6-di-tert-butyl-9H-carbazol-9-yl)phenoxy)methyl]benzaldehyde (1620641-13-5) + 5-(mesityl)dipyrromethane (159152-14-4) → 5,15-bis(2,4,6-trimethylphenyl)-10,20-bis[4-(4-(3,6-di-tert-butyl-9H-carbazol-9-yl)phenoxy)methylphenyl]porphyrin

Guidance literature:

4-[(4-(3,6-di-tert-butyl-9H-carbazol-9-yl)phenoxy)methyl]benzaldehyde; 5-(mesityl)dipyrromethane; With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

With chloranil; In dichloromethane; for 1h; Reflux; Inert atmosphere;

DOI:10.1039/c3ra45660a

upstream raw materials:

4-(3,6-di-tert-butyl-9H-carbazol-9-yl)phenol

4-(bromomethyl)benzaldehyde