4-N-acetylamino-1,2-benzenediol diacetate

Base Information

Chemical Name:4-N-acetylamino-1,2-benzenediol diacetate
CAS No.:74332-02-8
Molecular Formula:C₁₂H₁₃NO₅
Molecular Weight:251.239
Hs Code.:

Synonyms:4-N-acetylamino-1,2-benzenediol diacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-N-acetylamino-1,2-benzenediol diacetate

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 4-N-acetylamino-1,2-benzenediol diacetate

There total 8 articles about 4-N-acetylamino-1,2-benzenediol diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 6317-89-1
3-acetamidophenyl acetate

: 64-19-7,77671-22-8
acetic acid

: 74332-02-8
4-N-acetylamino-1,2-benzenediol diacetate

Guidance literature:: With boron trifluoride diethyl etherate; bis-[(trifluoroacetoxy)iodo]benzene; at 20 ℃; for 0.5h; regioselective reaction;
DOI:10.1039/c0ob00749h

Reference yield:

: 36383-33-2
4-nitro-1,2-benzenediol diacetate

: 74332-02-8
4-N-acetylamino-1,2-benzenediol diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / 10percent palladium-carbon / ethanol / 2.5 h / 2068.6 Torr

2: 0.65 g / 21 h

With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/0022-328X(95)05717-4

Reference yield:

: 13047-04-6
4-amino-1,2-benzenediol

: 74332-02-8
4-N-acetylamino-1,2-benzenediol diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: air / H₂O / pH 7.8

2: 1) NaBH₄ / 2) pyridine, 50 deg C, 2 h

With sodium tetrahydroborate; air; In water;
DOI:10.1021/jo01305a046