1,3-DITHIOLANE, 2-METHYL-2-(p-TOLYL)-

Base Information

Chemical Name:1,3-DITHIOLANE, 2-METHYL-2-(p-TOLYL)-
CAS No.:41159-08-4
Molecular Formula:C11H14S2
Molecular Weight:210.364
Hs Code.:
DSSTox Substance ID:DTXSID40194093
Nikkaji Number:J91.187I
Wikidata:Q83066848

Synonyms:BRN 4309664;2-Methyl-2-(p-tolyl)-1,3-dithiolane;1,3-DITHIOLANE, 2-METHYL-2-(p-TOLYL)-;41159-08-4;SCHEMBL2084258;DTXSID40194093;LS-63295

Suppliers and Price of 1,3-DITHIOLANE, 2-METHYL-2-(p-TOLYL)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 1,3-DITHIOLANE, 2-METHYL-2-(p-TOLYL)-

Chemical Property:

Vapor Pressure:0.000478mmHg at 25°C
Boiling Point:324°C at 760 mmHg
Flash Point:151.9°C
Density:1.127g/cm³
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:210.05369279
Heavy Atom Count:13
Complexity:165

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C2(SCCS2)C

Technology Process of 1,3-DITHIOLANE, 2-METHYL-2-(p-TOLYL)-

There total 3 articles about 1,3-DITHIOLANE, 2-METHYL-2-(p-TOLYL)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 540-63-6
ethane-1,2-dithiol

: 122-00-9
para-methylacetophenone

: 41159-08-4
2-methyl-2-(4-methylphenyl)-2-methyl-1,3-dithiolane

Guidance literature:: With silica gel; toluene-4-sulfonic acid; In dichloromethane; for 27h; Heating;
DOI:10.1055/s-2005-865303

Reference yield:

: 56637-45-7
2-methyl-2-(4-methylphenyl)-1,3-dithiane

: 41159-08-4
2-methyl-2-(4-methylphenyl)-2-methyl-1,3-dithiolane

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / 2,4,6-tris(p-chlorophenyl)pyrylium perchlorate, oxygen / CH₂Cl₂ / 1.67 h / Irradiation

2: FeCl₃-silica gel / CH₂Cl₂ / Ambient temperature

With oxygen; silica gel; iron(III) chloride; 2,4,6-tris(p-chlorophenyl)pyrylium perchlorate; In dichloromethane;
DOI:10.1016/S0040-4020(01)81203-5

Reference yield:

: 122-00-9
para-methylacetophenone

: 41159-08-4
2-methyl-2-(4-methylphenyl)-2-methyl-1,3-dithiolane

Guidance literature:: Multi-step reaction with 3 steps

1: FeCl₃-silica gel / CH₂Cl₂ / Ambient temperature

2: 72 percent / 2,4,6-tris(p-chlorophenyl)pyrylium perchlorate, oxygen / CH₂Cl₂ / 1.67 h / Irradiation

3: FeCl₃-silica gel / CH₂Cl₂ / Ambient temperature

With oxygen; silica gel; iron(III) chloride; 2,4,6-tris(p-chlorophenyl)pyrylium perchlorate; In dichloromethane;
DOI:10.1016/S0040-4020(01)81203-5