S-8-oxo-8-(phenylamino)octyl ethanethioate

Base Information

Chemical Name:S-8-oxo-8-(phenylamino)octyl ethanethioate
CAS No.:329966-80-5
Molecular Formula:C₁₆H₂₃NO₂S
Molecular Weight:293.43
Hs Code.:

Synonyms:S-8-oxo-8-(phenylamino)octyl ethanethioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-8-oxo-8-(phenylamino)octyl ethanethioate

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Technology Process of S-8-oxo-8-(phenylamino)octyl ethanethioate

There total 2 articles about S-8-oxo-8-(phenylamino)octyl ethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73674-09-6
8-bromo-n-octanoyl chloride

: 329966-80-5
S-8-oxo-8-(phenylamino)octyl ethanethioate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 20 °C

2: ethanol / 20 °C

With triethylamine; In ethanol; dichloromethane;
DOI:10.1021/jm049207j

Reference yield:

: 123-99-9,26776-28-3
azelaic acid

: 329966-80-5
S-8-oxo-8-(phenylamino)octyl ethanethioate

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene-4-sulfonic acid / toluene / 8 h / Reflux

2.1: sodium hydroxide / ethanol / 1 h / 20 °C

3.1: potassium hydroxide; silver nitrate / water / 0.33 h / 20 °C

3.2: 1.5 h / Cooling with ice

4.1: water; sodium hydroxide / 2 h / 45 °C

5.1: thionyl chloride / 1 h / Reflux

6.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Cooling with ice

7.1: ethanol / 20 h / 20 °C

With thionyl chloride; water; toluene-4-sulfonic acid; silver nitrate; triethylamine; potassium hydroxide; sodium hydroxide; In ethanol; dichloromethane; water; toluene;
DOI:10.1007/s00044-011-9879-7