4-(4-methoxybenzyl)-3,4-dihydro-1H-pyrido[3,2-e][1,4]diazepine-2,5-dione

Base Information

Chemical Name:4-(4-methoxybenzyl)-3,4-dihydro-1H-pyrido[3,2-e][1,4]diazepine-2,5-dione
CAS No.:1437787-07-9
Molecular Formula:C₁₆H₁₅N₃O₃
Molecular Weight:297.313
Hs Code.:

Synonyms:4-(4-methoxybenzyl)-3,4-dihydro-1H-pyrido[3,2-e][1,4]diazepine-2,5-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4-methoxybenzyl)-3,4-dihydro-1H-pyrido[3,2-e][1,4]diazepine-2,5-dione

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Technology Process of 4-(4-methoxybenzyl)-3,4-dihydro-1H-pyrido[3,2-e][1,4]diazepine-2,5-dione

There total 1 articles about 4-(4-methoxybenzyl)-3,4-dihydro-1H-pyrido[3,2-e][1,4]diazepine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 60857-16-1
N-(4-methoxybenzyl)glycine ethyl ester

: 63016-85-3
2H-pyrido[3,2-d][1,3]oxazine-2,4-(1H)-dione

: 1437787-07-9
4-(4-methoxybenzyl)-3,4-dihydro-1H-pyrido[3,2-e][1,4]diazepine-2,5-dione

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 18h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2013.04.089

Reference yield: 95.0%

: 1437787-07-9
4-(4-methoxybenzyl)-3,4-dihydro-1H-pyrido[3,2-e][1,4]diazepine-2,5-dione

: 1437787-10-4
4-(4-methoxybenzyl)-2-thioxo-3,4-dihydro-1H-pyrido[3,2-e][1,4]diazepin-5(2H)-one

Guidance literature:: With Lawessons reagent; In tetrahydrofuran; at 100 ℃; for 2h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2013.04.089

Reference yield:

: 1437787-07-9
4-(4-methoxybenzyl)-3,4-dihydro-1H-pyrido[3,2-e][1,4]diazepine-2,5-dione

: 1437787-25-1
2-(4-Benzylpiperazin-1-yl)-4-(4-methoxybenzyl)-3H-pyrido[3,2-e][1,4]diazepin-5(4H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: Lawessons reagent / tetrahydrofuran / 2 h / 100 °C / Inert atmosphere

2: mercury dichloride / tetrahydrofuran / 1 h / 100 °C / Inert atmosphere

With Lawessons reagent; mercury dichloride; In tetrahydrofuran;
DOI:10.1016/j.tet.2013.04.089