dibenzyl 2-(2-(benzyloxy(4-dibenzylphosphobutyl)amino)-2-oxoethyl)malonate

Base Information

Chemical Name:dibenzyl 2-(2-(benzyloxy(4-dibenzylphosphobutyl)amino)-2-oxoethyl)malonate
CAS No.:1360537-59-2
Molecular Formula:C₄₄H₄₆NO₁₀P
Molecular Weight:779.824
Hs Code.:

Synonyms:dibenzyl 2-(2-(benzyloxy(4-dibenzylphosphobutyl)amino)-2-oxoethyl)malonate

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Chemical Property of dibenzyl 2-(2-(benzyloxy(4-dibenzylphosphobutyl)amino)-2-oxoethyl)malonate

Chemical Property:

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Technology Process of dibenzyl 2-(2-(benzyloxy(4-dibenzylphosphobutyl)amino)-2-oxoethyl)malonate

There total 5 articles about dibenzyl 2-(2-(benzyloxy(4-dibenzylphosphobutyl)amino)-2-oxoethyl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₄₆NO₉P

: 1360537-59-2
dibenzyl 2-(2-(benzyloxy(4-dibenzylphosphobutyl)amino)-2-oxoethyl)malonate

Guidance literature:: With tert.-butylhydroperoxide; In water; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2011.12.050

Reference yield:

: 15014-25-2
malonic acid dibenzyl ester

: 1360537-59-2
dibenzyl 2-(2-(benzyloxy(4-dibenzylphosphobutyl)amino)-2-oxoethyl)malonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 0 - 20 °C

2.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

4.1: triethylamine / methanol; dichloromethane / 0 - 20 °C

5.1: 1H-imidazole; 1,2,4-Triazole / dichloromethane / 20 °C / Inert atmosphere

6.1: tert.-butylhydroperoxide / water / 0 - 20 °C

With 1H-imidazole; 1,2,4-Triazole; tert.-butylhydroperoxide; oxalyl dichloride; sodium hydride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.12.050

Reference yield:

: 289637-26-9
dibenzyl 2-carboxymethylmalonate

: 1360537-59-2
dibenzyl 2-(2-(benzyloxy(4-dibenzylphosphobutyl)amino)-2-oxoethyl)malonate

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

2: triethylamine / methanol; dichloromethane / 0 - 20 °C

3: 1H-imidazole; 1,2,4-Triazole / dichloromethane / 20 °C / Inert atmosphere

4: tert.-butylhydroperoxide / water / 0 - 20 °C

With 1H-imidazole; 1,2,4-Triazole; tert.-butylhydroperoxide; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In methanol; dichloromethane; water;
DOI:10.1016/j.bmc.2011.12.050