C₃₄H₄₉N₅O₉

Base Information

Chemical Name:C₃₄H₄₉N₅O₉
CAS No.:1335123-03-9
Molecular Formula:C₃₄H₄₉N₅O₉
Molecular Weight:671.791
Hs Code.:

C<sub>34</sub>H<sub>49</sub>N<sub>5</sub>O<sub>9</sub>

Synonyms:C₃₄H₄₉N₅O₉

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Chemical Property of C₃₄H₄₉N₅O₉

Chemical Property:

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Technology Process of C₃₄H₄₉N₅O₉

There total 6 articles about C₃₄H₄₉N₅O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1186120-58-0
tert-butyl(1S,2S)-3-azido-1-hydroxy-1-(4-nitrophenyl)propan-2-ylcarbamate

: 1335123-03-9
C₃₄H₄₉N₅O₉

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine / tetrahydrofuran; water / 24 h / 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmc.2011.07.008

Reference yield:

: 1186120-57-9
tert-butyl (1S,2R)-3-bromo-1-hydroxy-1-(4-nitrophenyl)propan-2-ylcarbamate

: 1335123-03-9
C₃₄H₄₉N₅O₉

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / N,N-dimethyl-formamide / 12 h / 65 °C / Inert atmosphere

2: triphenylphosphine / tetrahydrofuran; water / 24 h / 20 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

With sodium azide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.07.008

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1335123-03-9
C₃₄H₄₉N₅O₉

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / 24 h / 20 °C

2: N-Bromosuccinimide; triphenylphosphine / tetrahydrofuran / 9.5 h / 0 - 20 °C

3: sodium azide / N,N-dimethyl-formamide / 12 h / 65 °C / Inert atmosphere

4: triphenylphosphine / tetrahydrofuran; water / 24 h / 20 °C

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

With N-Bromosuccinimide; sodium azide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.07.008