{3-methyl-2-(2-propyl)-1-butene}{bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾

Base Information

• Chemical Name: {3-methyl-2-(2-propyl)-1-butene}{bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾
• CAS No.: 111848-52-3
• Molecular Formula: C₃₄H₆₄P₂Pt
• Molecular Weight: 729.91

Synonyms:{3-methyl-2-(2-propyl)-1-butene}{bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾

Chemical Property of {3-methyl-2-(2-propyl)-1-butene}{bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾

Chemical Property:

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Technology Process of {3-methyl-2-(2-propyl)-1-butene}{bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾

There total 2 articles about {3-methyl-2-(2-propyl)-1-butene}{bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

cis-[bis-(dicyclohexylphosphino)ethane]hydridoneopentylplatinum(II) + 3-methyl-2-isopropyl-1-butene (111823-35-9) → {3-methyl-2-(2-propyl)-1-butene}{bis(dicyclohexylphosphino)ethane}platinum(0) (111848-52-3) + 2,2-dimethylpropane (463-82-1)

Guidance literature:

In cyclohexane; thermolysis of cis-hydridoneopentyl{bis(dicyclohexylphosphino)ethane}platinum(II) in 3-methyl-2-(2-propyl)-1-butene/cyclohexane via supposed {bis(dicyclohexylphosphino)ethane}platinum(0) at 69°C to completion; Kinetics;

DOI:10.1021/ja00213a016

Reference yield: 21.0%

cis-[bis-(dicyclohexylphosphino)ethane]hydridoneopentylplatinum(II) + 3-methyl-2-isopropyl-1-butene (111823-35-9) → {3-methyl-2-(2-propyl)-1-butene}{bis(dicyclohexylphosphino)ethane}platinum(0) (111848-52-3)

Guidance literature:

In cyclohexane; cis-hydridoneopentyl{bis(dicyclohexylphosphino)ethane}platinum(II) in 3-methyl-2-(2-propyl)-1-butene/cyclohexane vacuum-sealed and heated at 69°C for 2.5 h, opened, solvent evapd., dissolved in min. hexane; solvent evapd. under Ar until crystn., addnl. crop at -10°C, washed with cold hexane;

DOI:10.1021/ja00213a016

upstream raw materials:

3-methyl-2-isopropyl-1-butene

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