11-azidoundecyl O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:11-azidoundecyl O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:709040-94-8
Molecular Formula:C₅₈H₇₃N₃O₁₁
Molecular Weight:988.231
Hs Code.:

Synonyms:11-azidoundecyl O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Suppliers and Price of 11-azidoundecyl O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 11-azidoundecyl O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 11-azidoundecyl O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 8 articles about 11-azidoundecyl O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 709040-91-5
11-azidoundecyl O-(2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 709040-94-8
11-azidoundecyl O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With acetic acid; at 85 ℃;
DOI:10.1039/b400029c

Reference yield:

: 61198-91-2
2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide

: 709040-94-8
11-azidoundecyl O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1.1: 4 Angstroem molecular sieves / toluene / -78 °C

1.2: silver triflate / toluene / 1 h / -78 - 10 °C

2.1: 3.36 g / NaOMe / methanol / Heating

3.1: 87 percent / CSA / Heating

4.1: NaH / dimethylformamide / 0.5 h

4.2: 92 percent / dimethylformamide / 2 h / 20 °C

5.1: 96 percent / aq. AcOH / 85 °C

With 4 A molecular sieve; camphor-10-sulfonic acid; sodium methylate; sodium hydride; acetic acid; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1039/b400029c

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 709040-94-8
11-azidoundecyl O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: 96 percent / NaN₃ / dimethylformamide / 50 h / 100 - 130 °C

2.1: 4 Angstroem molecular sieves / toluene / -78 °C

2.2: silver triflate / toluene / 1 h / -78 - 10 °C

3.1: 3.36 g / NaOMe / methanol / Heating

4.1: 87 percent / CSA / Heating

5.1: NaH / dimethylformamide / 0.5 h

5.2: 92 percent / dimethylformamide / 2 h / 20 °C

6.1: 96 percent / aq. AcOH / 85 °C

With sodium azide; 4 A molecular sieve; camphor-10-sulfonic acid; sodium methylate; sodium hydride; acetic acid; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1039/b400029c