Technology Process of C26H26N2O7
There total 7 articles about C26H26N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4-methyl-2-nitrophenol;
With
potassium hydroxide;
In
ethanol; water;
C26H27NO7S;
In
ethanol; water; N,N-dimethyl-formamide;
at 120 ℃;
for 12h;
Inert atmosphere;
DOI:10.1039/c3cc42489h
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium hydroxide / ethanol / 12 h / 20 °C
2.1: nitric acid / acetic acid / 12 h / 50 °C / Cooling with ice
3.1: trifluoroacetic acid / dichloromethane / 48 h / 20 °C
4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 72 h / 100 °C / Inert atmosphere
5.1: dmap / dichloromethane / 12 h / 0 - 20 °C
6.1: potassium hydroxide / ethanol; water
6.2: 12 h / 120 °C / Inert atmosphere
With
dmap; nitric acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; potassium hydroxide;
In
ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/c3cc42489h
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium hydroxide / ethanol / 12 h / 20 °C
2.1: nitric acid / acetic acid / 12 h / 50 °C / Cooling with ice
3.1: trifluoroacetic acid / dichloromethane / 48 h / 20 °C
4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 72 h / 100 °C / Inert atmosphere
5.1: dmap / dichloromethane / 12 h / 0 - 20 °C
6.1: potassium hydroxide / ethanol; water
6.2: 12 h / 120 °C / Inert atmosphere
With
dmap; nitric acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; potassium hydroxide;
In
ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/c3cc42489h
