C₁₂H₁₅NO₂

Base Information

Chemical Name:C₁₂H₁₅NO₂
CAS No.:1237739-84-2
Molecular Formula:C₁₂H₁₅NO₂
Molecular Weight:205.257
Hs Code.:

C<sub>12</sub>H<sub>15</sub>NO<sub>2</sub>

Synonyms:C₁₂H₁₅NO₂

Suppliers and Price of C₁₂H₁₅NO₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₅NO₂

Chemical Property:

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Technology Process of C₁₂H₁₅NO₂

There total 3 articles about C₁₂H₁₅NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57690-96-7
2,2-dimethylbut-3-enoyl chloride

: 100-65-2
N-Phenylhydroxylamine

: 1237739-84-2
C₁₂H₁₅NO₂

Guidance literature:: With sodium hydrogencarbonate; In ethanol; water; at 0 ℃; Inert atmosphere;
DOI:10.1002/anie.201000843

Reference yield:

: 10276-09-2
2,2-dimethyl-but-3-enoic acid

: 1237739-84-2
C₁₂H₁₅NO₂

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 0.92 h / 0 - 20 °C / Inert atmosphere

2: diethyl ether; water / 0 °C

With oxalyl dichloride; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja204255e

Reference yield:

: 80-59-1
Tiglic acid

: 1237739-84-2
C₁₂H₁₅NO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; diethylamine / tetrahydrofuran; hexane / -78 - 0 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 0.92 h / 0 - 20 °C / Inert atmosphere

3.1: diethyl ether; water / 0 °C

With n-butyllithium; oxalyl dichloride; diethylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja204255e