-5-(2-benzoylvinyl)-2,4-dimethoxypyrimidine

Base Information

Chemical Name:-5-(2-benzoylvinyl)-2,4-dimethoxypyrimidine
CAS No.:130749-66-5
Molecular Formula:C₁₅H₁₄N₂O₃
Molecular Weight:270.288
Hs Code.:

<E>-5-(2-benzoylvinyl)-2,4-dimethoxypyrimidine

Synonyms:-5-(2-benzoylvinyl)-2,4-dimethoxypyrimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of -5-(2-benzoylvinyl)-2,4-dimethoxypyrimidine

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Technology Process of -5-(2-benzoylvinyl)-2,4-dimethoxypyrimidine

There total 7 articles about -5-(2-benzoylvinyl)-2,4-dimethoxypyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 130749-58-5
5-(3-hydroxy-3-phenyl-prop-1-enyl)-2,4-dimethoxypyrimidine

: 130749-66-5
-5-(2-benzoylvinyl)-2,4-dimethoxypyrimidine

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 28 - 30 ℃; for 16h;

Reference yield:

: 4393-06-0
1-Phenyl-2-propen-1-ol

: 130749-66-5
-5-(2-benzoylvinyl)-2,4-dimethoxypyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Jones' reagent / acetone / 0.5 h / 0 °C

2: 29 percent / bis(triphenylphosphine) palladium(II)chloride, CuI, Et₃N / 24 h / Heating

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; jones' reagent; triethylamine; In acetone;
DOI:10.1016/0223-5234(93)90015-7

Reference yield:

: 4187-87-5
1-Phenyl-2-propyn-1-ol

: 130749-66-5
-5-(2-benzoylvinyl)-2,4-dimethoxypyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / LAH / diethyl ether / 18 h / Ambient temperature

2: 80 percent / Jones' reagent / acetone / 0.5 h / 0 °C

3: 29 percent / bis(triphenylphosphine) palladium(II)chloride, CuI, Et₃N / 24 h / Heating

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium aluminium tetrahydride; jones' reagent; triethylamine; In diethyl ether; acetone;
DOI:10.1016/0223-5234(93)90015-7