sodium 2-((1-(2-ethoxy-2-oxoethyl)-5-fluoro-2-methyl-1H-indol-3-yl)methyl)benzenesulfonate

Base Information

Chemical Name:sodium 2-((1-(2-ethoxy-2-oxoethyl)-5-fluoro-2-methyl-1H-indol-3-yl)methyl)benzenesulfonate
CAS No.:1174009-28-9
Molecular Formula:C₂₀H₁₉FNO₅S*Na
Molecular Weight:427.429
Hs Code.:

Synonyms:sodium 2-((1-(2-ethoxy-2-oxoethyl)-5-fluoro-2-methyl-1H-indol-3-yl)methyl)benzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium 2-((1-(2-ethoxy-2-oxoethyl)-5-fluoro-2-methyl-1H-indol-3-yl)methyl)benzenesulfonate

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Technology Process of sodium 2-((1-(2-ethoxy-2-oxoethyl)-5-fluoro-2-methyl-1H-indol-3-yl)methyl)benzenesulfonate

There total 1 articles about sodium 2-((1-(2-ethoxy-2-oxoethyl)-5-fluoro-2-methyl-1H-indol-3-yl)methyl)benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 851460-85-0
(5-fluoro-2-methylindol-1-yl)-acetic acid ethyl ester

: 1008-72-6
sodium 2-formylbenzenesulfonate

: 1174009-28-9
sodium 2-((1-(2-ethoxy-2-oxoethyl)-5-fluoro-2-methyl-1H-indol-3-yl)methyl)benzenesulfonate

Guidance literature:: (5-fluoro-2-methylindol-1-yl)-acetic acid ethyl ester; sodium 2-formylbenzenesulfonate; With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 72.5h;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield: 89.0%

: 1174009-28-9
sodium 2-((1-(2-ethoxy-2-oxoethyl)-5-fluoro-2-methyl-1H-indol-3-yl)methyl)benzenesulfonate

: 1174009-29-0
ethyl 2-(3-(2-(chlorosulfonyl)benzyl)-5-fluoro-2-methyl-1H-indol-1-yl)acetate

Guidance literature:: With chlorosulfonic acid; at 20 ℃; for 2.33333h;

Reference yield:

: 1174009-28-9
sodium 2-((1-(2-ethoxy-2-oxoethyl)-5-fluoro-2-methyl-1H-indol-3-yl)methyl)benzenesulfonate

: 1155694-69-1
2-(5-fluoro-2-methyl-3-(2-(piperidin-1-ylsulfonyl)benzyl)-1H-indol-1-yl)acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: chlorosulfonic acid / 2.33 h / 20 °C

2: pyridine / 18 h / 20 °C

3: water; potassium hydroxide / tetrahydrofuran / 2 h / 20 °C

With pyridine; chlorosulfonic acid; water; potassium hydroxide; In tetrahydrofuran;