C₂₈H₄₁NO₄Si

Base Information

Chemical Name:C₂₈H₄₁NO₄Si
CAS No.:1543007-29-9
Molecular Formula:C₂₈H₄₁NO₄Si
Molecular Weight:483.723
Hs Code.:

C<sub>28</sub>H<sub>41</sub>NO<sub>4</sub>Si

Synonyms:C₂₈H₄₁NO₄Si

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Chemical Property of C₂₈H₄₁NO₄Si

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Technology Process of C₂₈H₄₁NO₄Si

There total 13 articles about C₂₈H₄₁NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1543006-66-1
tert-butyl (2R,3S)-2-(2-(benzyloxy)ethyl)-3-((tert-butyldiphenylsilyloxy)methyl)pyrrolidine-1-carboxylate

: 1543007-29-9
C₂₈H₄₁NO₄Si

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 6h;
DOI:10.1016/j.tet.2013.12.078

Reference yield:

: 1543006-73-0
(2R,3S)-2-allyl-5-(benzyloxy)pentane-1,3-diol

: 1543007-29-9
C₂₈H₄₁NO₄Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: camphor-10-sulfonic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; toluene / 4 h / 20 °C / Inert atmosphere

3.1: sodium periodate / tetrahydrofuran; aq. phosphate buffer / 0.75 h / 0 °C / pH Ca_. 7 / Inert atmosphere

4.1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

5.1: triethylamine; dmap / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

6.1: sodium azide / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

7.1: acetic acid; water / 3 h / 100 °C / Inert atmosphere

8.1: triethylamine; dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

9.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

10.1: triphenylphosphine / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

10.2: 36 h / Inert atmosphere; Reflux

11.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

12.1: palladium 10% on activated carbon; hydrogen / methanol / 6 h

With dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; sodium azide; palladium 10% on activated carbon; camphor-10-sulfonic acid; water; hydrogen; acetic acid; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; aq. phosphate buffer; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.tet.2013.12.078

Reference yield:

: 1543006-77-4
(4S,5R)-5-allyl-4-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxane

: 1543007-29-9
C₂₈H₄₁NO₄Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; toluene / 4 h / 20 °C / Inert atmosphere

2.1: sodium periodate / tetrahydrofuran; aq. phosphate buffer / 0.75 h / 0 °C / pH Ca_. 7 / Inert atmosphere

3.1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

4.1: triethylamine; dmap / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

5.1: sodium azide / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

6.1: acetic acid; water / 3 h / 100 °C / Inert atmosphere

7.1: triethylamine; dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

8.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

9.1: triphenylphosphine / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

9.2: 36 h / Inert atmosphere; Reflux

10.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

11.1: palladium 10% on activated carbon; hydrogen / methanol / 6 h

With dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; sodium azide; palladium 10% on activated carbon; water; hydrogen; acetic acid; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; aq. phosphate buffer; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.tet.2013.12.078