2-(2-Trifluoroacetylimino-6-trifluoromethoxy-3-benzothiazolinyl)ethyl para-toluenesulphonate

Base Information

Chemical Name:2-(2-Trifluoroacetylimino-6-trifluoromethoxy-3-benzothiazolinyl)ethyl para-toluenesulphonate
CAS No.:130997-83-0
Molecular Formula:C₁₉H₁₄F₆N₂O₅S₂
Molecular Weight:528.453
Hs Code.:

Synonyms:2-(2-Trifluoroacetylimino-6-trifluoromethoxy-3-benzothiazolinyl)ethyl para-toluenesulphonate

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Chemical Property of 2-(2-Trifluoroacetylimino-6-trifluoromethoxy-3-benzothiazolinyl)ethyl para-toluenesulphonate

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Technology Process of 2-(2-Trifluoroacetylimino-6-trifluoromethoxy-3-benzothiazolinyl)ethyl para-toluenesulphonate

There total 4 articles about 2-(2-Trifluoroacetylimino-6-trifluoromethoxy-3-benzothiazolinyl)ethyl para-toluenesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 98-59-9
p-toluenesulfonyl chloride

: 130997-84-1
2,2,2-trifluoro-N-[3-(2-hydroxy-ethyl)-6-trifluoromethoxy-3H-benzothiazol-2-ylidene]-acetamide

: 130997-83-0
2-(2-Trifluoroacetylimino-6-trifluoromethoxy-3-benzothiazolinyl)ethyl para-toluenesulphonate

Guidance literature:: With pyridine; Ambient temperature;
DOI:10.1021/jm980202u

Reference yield:

: 461-82-5
4-(trifluoromethoxy)aniline

: 130997-83-0
2-(2-Trifluoroacetylimino-6-trifluoromethoxy-3-benzothiazolinyl)ethyl para-toluenesulphonate

Guidance literature:: Multi-step reaction with 4 steps

1: Br₂, AcOH / 21 h / Ambient temperature

2: butan-2-one / 24 h / Heating

3: 85 percent / Et₃N / ethanol / Ambient temperature

4: 90 percent / pyridine / Ambient temperature

With pyridine; bromine; acetic acid; triethylamine; In ethanol; butanone;
DOI:10.1021/jm980202u

Reference yield:

: 133783-55-8
3-(2-hydroxyethyl)-2-imino-6-trifluoromethoxybenzothiazoline

: 130997-83-0
2-(2-Trifluoroacetylimino-6-trifluoromethoxy-3-benzothiazolinyl)ethyl para-toluenesulphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Et₃N / ethanol / Ambient temperature

2: 90 percent / pyridine / Ambient temperature

With pyridine; triethylamine; In ethanol;
DOI:10.1021/jm980202u