4-butyloxy-3-methoxybenzophenone-(E)-3,5-dimethoxycarbonylphenylsulfohydrazone

Base Information

Chemical Name:4-butyloxy-3-methoxybenzophenone-(E)-3,5-dimethoxycarbonylphenylsulfohydrazone
CAS No.:926291-99-8
Molecular Formula:C₂₈H₃₀N₂O₈S
Molecular Weight:554.621
Hs Code.:

Synonyms:4-butyloxy-3-methoxybenzophenone-(E)-3,5-dimethoxycarbonylphenylsulfohydrazone

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Chemical Property of 4-butyloxy-3-methoxybenzophenone-(E)-3,5-dimethoxycarbonylphenylsulfohydrazone

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Technology Process of 4-butyloxy-3-methoxybenzophenone-(E)-3,5-dimethoxycarbonylphenylsulfohydrazone

There total 4 articles about 4-butyloxy-3-methoxybenzophenone-(E)-3,5-dimethoxycarbonylphenylsulfohydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 926291-89-6
5-hydrazosulfonylbenzene-1,3-carboxylic acid dimethyl ester

: 926291-93-2
4-butyloxy-3-methoxybenzophenone

: 926291-99-8
4-butyloxy-3-methoxybenzophenone-(E)-3,5-dimethoxycarbonylphenylsulfohydrazone

Guidance literature:: In methanol; for 18h; Heating;
DOI:10.1021/jm060834d

Reference yield:

: 51439-89-5
(4-hydroxy-3-methoxyphenyl)(phenyl)methanone

: 926291-99-8
4-butyloxy-3-methoxybenzophenone-(E)-3,5-dimethoxycarbonylphenylsulfohydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Na₂CO₃ / dimethylformamide / 2 h / 80 °C

2: 91 percent / methanol / 18 h / Heating

With sodium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm060834d

Reference yield:

: sodium 3,5-bis(methoxycarbonyl)benzenesulfonic acid

: 926291-99-8
4-butyloxy-3-methoxybenzophenone-(E)-3,5-dimethoxycarbonylphenylsulfohydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / PCl₅; diisopropylamine / CCl₄ / 6 h / Heating

2: 56 percent / hydrazine hydrate / ethanol; CHCl₃ / 6 h

3: 91 percent / methanol / 18 h / Heating

With phosphorus pentachloride; hydrazine hydrate; diisopropylamine; In methanol; tetrachloromethane; ethanol; chloroform;
DOI:10.1021/jm060834d