2,6-anhydro-3,4,5-tri-O-benzyl-7-O-tert-butyldiphenylsilyl-aldehydo-D-glycero-L-manno-heptose

Base Information

Chemical Name:2,6-anhydro-3,4,5-tri-O-benzyl-7-O-tert-butyldiphenylsilyl-aldehydo-D-glycero-L-manno-heptose
CAS No.:216485-34-6
Molecular Formula:C₄₄H₄₈O₆Si
Molecular Weight:700.947
Hs Code.:

Synonyms:2,6-anhydro-3,4,5-tri-O-benzyl-7-O-tert-butyldiphenylsilyl-aldehydo-D-glycero-L-manno-heptose

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Chemical Property of 2,6-anhydro-3,4,5-tri-O-benzyl-7-O-tert-butyldiphenylsilyl-aldehydo-D-glycero-L-manno-heptose

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Technology Process of 2,6-anhydro-3,4,5-tri-O-benzyl-7-O-tert-butyldiphenylsilyl-aldehydo-D-glycero-L-manno-heptose

There total 6 articles about 2,6-anhydro-3,4,5-tri-O-benzyl-7-O-tert-butyldiphenylsilyl-aldehydo-D-glycero-L-manno-heptose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-Methyl-2-[(2R,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-2-yl]-2,3-dihydro-benzothiazole

: 216485-34-6
2,6-anhydro-3,4,5-tri-O-benzyl-7-O-tert-butyldiphenylsilyl-aldehydo-D-glycero-L-manno-heptose

Guidance literature:: With silver nitrate; In dichloromethane; acetonitrile; at 20 ℃; for 0.25h;
DOI:10.1021/jo011142u

Reference yield:

: 160797-12-6
2-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-1,3-thiazole

: 216485-34-6
2,6-anhydro-3,4,5-tri-O-benzyl-7-O-tert-butyldiphenylsilyl-aldehydo-D-glycero-L-manno-heptose

Guidance literature:: Multi-step reaction with 4 steps

1: H₂SO₄ / acetic acid / Ambient temperature

2: MeONa / methanol / Ambient temperature

3: pyridine / Ambient temperature

With pyridine; sulfuric acid; sodium methylate; In methanol; acetic acid;
DOI:10.1016/S0040-4039(98)01739-0

Reference yield:

: Acetic acid (2R,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-thiazol-2-yl-tetrahydro-pyran-2-ylmethyl ester

: 216485-34-6
2,6-anhydro-3,4,5-tri-O-benzyl-7-O-tert-butyldiphenylsilyl-aldehydo-D-glycero-L-manno-heptose

Guidance literature:: Multi-step reaction with 3 steps

1: MeONa / methanol / Ambient temperature

2: pyridine / Ambient temperature

With pyridine; sodium methylate; In methanol;
DOI:10.1016/S0040-4039(98)01739-0