(2R,3R,4R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-5-phenylsulfanyl-tetrahydro-furan

Base Information

Chemical Name:(2R,3R,4R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-5-phenylsulfanyl-tetrahydro-furan
CAS No.:149118-07-0
Molecular Formula:C₃₂H₃₂O₄S
Molecular Weight:512.67
Hs Code.:

Synonyms:(2R,3R,4R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-5-phenylsulfanyl-tetrahydro-furan

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Chemical Property of (2R,3R,4R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-5-phenylsulfanyl-tetrahydro-furan

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Technology Process of (2R,3R,4R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-5-phenylsulfanyl-tetrahydro-furan

There total 6 articles about (2R,3R,4R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-5-phenylsulfanyl-tetrahydro-furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 108-98-5
thiophenol

: 148623-62-5
2,3,5-tri-O-benzyl-1-O-methoxyacetyl-β-D-ribofuranose

: 149118-07-0
(2R,3R,4R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-5-phenylsulfanyl-tetrahydro-furan

Guidance literature:: ytterbium(III) triflate; In acetonitrile; at 23 ℃; for 1h;
DOI:10.1016/S0040-4039(00)73563-5

Reference yield: 96.0%

: 16838-89-4
2,3,5-tri-O-benzyl-D-ribofuranose

: 108-98-5
thiophenol

: 149118-07-0
(2R,3R,4R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-5-phenylsulfanyl-tetrahydro-furan

Guidance literature:: With 4 A molecular sieve; 2-methoxyacetic acid; ytterbium(III) triflate; In dichloromethane; for 1.5h; Heating;
DOI:10.1039/C39930001090

Reference yield: 92.0%

: 14365-16-3
bis-(phenylthio)-dibutylstannane

: 91110-24-6
Acetic acid (2S,3R,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yl ester

: 149118-07-0
(2R,3R,4R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-5-phenylsulfanyl-tetrahydro-furan

Guidance literature:: With di-n-butylbis(trifluoromethanesulfonyloxy)stannane; In 1,2-dichloro-ethane; at 50 ℃; for 2h;
DOI:10.1016/0040-4039(92)88060-I