2-<2-ethoxycarbonyl-3-(β-methoxyethoxymethoxy)-5-methoxyphenylmethyl>-2-(E-1-methylprop-1-enyl)-1,3-dithian

Base Information

Chemical Name:2-<2-ethoxycarbonyl-3-(β-methoxyethoxymethoxy)-5-methoxyphenylmethyl>-2-(E-1-methylprop-1-enyl)-1,3-dithian
CAS No.:74149-61-4
Molecular Formula:C₂₃H₃₄O₆S₂
Molecular Weight:470.651
Hs Code.:

Synonyms:2-<2-ethoxycarbonyl-3-(β-methoxyethoxymethoxy)-5-methoxyphenylmethyl>-2-(E-1-methylprop-1-enyl)-1,3-dithian

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Chemical Property of 2-<2-ethoxycarbonyl-3-(β-methoxyethoxymethoxy)-5-methoxyphenylmethyl>-2-(E-1-methylprop-1-enyl)-1,3-dithian

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Technology Process of 2-<2-ethoxycarbonyl-3-(β-methoxyethoxymethoxy)-5-methoxyphenylmethyl>-2-(E-1-methylprop-1-enyl)-1,3-dithian

There total 3 articles about 2-<2-ethoxycarbonyl-3-(β-methoxyethoxymethoxy)-5-methoxyphenylmethyl>-2-(E-1-methylprop-1-enyl)-1,3-dithian which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 74149-62-5
2-((E)-1-propenyl)-1,3-dithiane

: 343620-57-5
ethyl 2-(β-methoxyethoxymethoxy)-4-methoxy-6-bromomethylbenzoate

: 74149-61-4
2-<2-ethoxycarbonyl-3-(β-methoxyethoxymethoxy)-5-methoxyphenylmethyl>-2-(E-1-methylprop-1-enyl)-1,3-dithian

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) -20 deg C, 3 h, 2.) -78 deg C, few minutes;

Reference yield:

: 497-03-0
2-methylbut-2-enal

: 74149-61-4
2-<2-ethoxycarbonyl-3-(β-methoxyethoxymethoxy)-5-methoxyphenylmethyl>-2-(E-1-methylprop-1-enyl)-1,3-dithian

Guidance literature:: Multi-step reaction with 2 steps

1: BF₃-ether

2: 85 percent / n-butyl-lithium / hexane; tetrahydrofuran / 1.) -20 deg C, 3 h, 2.) -78 deg C, few minutes

With n-butyllithium; boron trifluoride diethyl etherate; In tetrahydrofuran; hexane;

Reference yield:

: 74149-60-3
2-bromomethyl-6-hydroxy-4-methoxy-benzoic acid ethyl ester

: 74149-61-4
2-<2-ethoxycarbonyl-3-(β-methoxyethoxymethoxy)-5-methoxyphenylmethyl>-2-(E-1-methylprop-1-enyl)-1,3-dithian

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran / 1.) -20 deg C, 30 min, 2.) -20 deg C, 15 h

2: 85 percent / n-butyl-lithium / hexane; tetrahydrofuran / 1.) -20 deg C, 3 h, 2.) -78 deg C, few minutes

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane;